Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.
NYC-WTC_000088700–000088724Folder label: “GC/MS Scan 9/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\LB.D Vial: 3 Acq On : 16 Oct 2001 4:11 pm Operator: 209 GALOS Sample : lab blk 9/27 Inst ; GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Tricosane Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 30.71 1.26 ug/1 134616 Chrysehe-dl2 33.12 it# of 5 Tentative ID MW MolForm CAS# Qual
Tricosane 324 C23H48 000638-67-5 95 2 Octadecane 254 C18H38 000593-45-3 91 3 Eicosane 282 C20H42 000112-95-8 91 4 Tetracosane 338 C24H50 000646-31-1 90 Abundance Scan 2796 (30.707 min): LB.D (-) m/z 57700 100.00% 57 43 71
85 5000 --rrT-p-rT-7-|-T/-iVp--rT-r*pT-r^^ 99 113 30.40 30.60 30.80 31.00 , y,, I , J,,, J ■J, .......................... m/z 71.10 74.29% TTfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #73318: Tricosane 4(3 5(7
71 5000 85 30,40 30.60 30.80 31.00 m/z 43705 71723% « I " I I I I 1 I I 1 I I I » . I I I 1 I I Y1 I I I 'i I I •' I T'l -I I I i‘ I I I I I I I I p-r. I I . I . . I . I I 1 I I I I ' ’ I' ''' I ‘' TiZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #71561: Octadecane
43 71 ~ : I l~ 1 I rj , . I r'|-r, i , , . r , ■ । . 30.40 30.60 30.80 31.00 85 5000 Wz 85.05 51.14%
99 J ' I ' ' * ' I ’ ‘ ' I ' ' ' ’ I I ' ' ’ ' I 224 -254 - ' I '''' I'''' I''' ' I''' ' I Ti/z-> Abundance 40 60
- 43 5 7 80 100 120 140 160 180 200 220 240 260 280 300 320 #39862: Eicosane .. £... 30.40 30.60 30.80 31.00 - 71 m/z 41705 28.89%
5000 85 J I II 3/113127141155 196 240 282 I I n I I f i I "p ITI I I I I I I I I I I I '' 1 7 1 11 , 1YI I , T f. I 1 1 f 1 I Tiyk-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 30.40 30.60 30.80 31.00
LB.D NP091101.M Thu Oct 18 10:43:51 2001 Page 7
NYC-WTC_000088712
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NYC-WTC_000089278
GC/MS calibration table listing compounds like 1,4-Dichlorobenzene-d4 and Naphthalene-d8 from October 2001.
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Instrument output displaying chromatographic peaks and integration parameters for a laboratory blank analyzed on October 12, 2001.
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Calibration table and chromatographic data for the TCLP method using GC/MS instrument 209, dated October 3, 2001.
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Laboratory data sheet listing extraction dates and calibration results for deuterated standards.
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GC/MS analysis report with TCLP calibration table data from October 16, 2001.
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Calibration data table for GC/MS analysis using the TCLP method, generated on October 3, 2001, listing standard compounds and response factors.
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Calibration data table for GC/MS analysis of WTC samples conducted on October 2, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23799 conducted on November 1, 2001, identifying unknown compounds.
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Laboratory report documenting GC/MS analysis of sample AD23503 conducted on October 19, 2001.
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machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000086624
Calibration data table for GC/MS analysis of polycyclic aromatic hydrocarbons dated October 2001.
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Laboratory report documenting GC/MS analysis of sample AD23836 conducted on November 1, 2001, identifying unknown compounds.
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Document containing tabular laboratory data including pH and count metrics for environmental sample analysis in November 2001.
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NYC-WTC_000088695
Gas chromatography-mass spectrometry scan results recorded on September 27, 2001 for environmental samples.
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NYC-WTC_000088696
Fragmented GC/MS scan page from a laboratory blank sample dated September 27, 2001.
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NYC-WTC_000088725
Laboratory report documenting GC/MS analysis of sample AD23473 conducted on October 19, 2001.
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Laboratory report documenting GC/MS analysis of sample AD23497 conducted on October 19, 2001.
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