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GC/MS calibration report for TCLP method, Oct 2001

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Instrument calibration report for GC/MS Method NP091101 used for TCLP analysis, generated on October 16, 2001.

NYC-WTC_000088700–000088724

Folder label: “GC/MS Scan 9/27/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\LB.D Vial: 3 Acq On : 16 Oct 2001 4:11 pm Operator: 209 GALOS Sample : lab blk 9/27 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Heptadecane Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 29.62 0.80 ug/1 85199 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForin CAS# Qual

1 Heptadecane 240 C17H36 000629-78-7 9K 2 Hexatriacontane 507 C36H74 000630-06-8 9y 3 Octadecane 254 C18H38 000593-45-3 9C) 4 Pentacosane 352 C25H52 000629-99-2 87 Abundance Scan 2678 (29.624 min): LB.D (-) m/z 57700 TOOTOO? 57 43 71 5000 85

'I 99 29,20 29,40 29,60 29,80 30,00 ■m/z 4^705 73.98% iT/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #71193: Heptadecane 57

71 5000 I-..................................................... 85 29,20 29,40 29,60 29,80 30,00 “mTz 71.00 65.76%

Abundance 40 1 T"*—J—m—r-r-m—[—tA—r 60 80 T 100 120 127 141 155 169 140 160 180 200 210 220 240 240 ft #74636: Hexatriacontane____ 43

71 JQu 29,20 29,40 29,60 29,80 30,00 5000 85 m/z 85.05 49731%

, || , 141 155 169 183" 197 211................... ..

■n/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #71560: Octadecane —43- 5(7 29,20 29,40 ,29,60 -29.80 r 30,00 - "mTz 41705 28.41% 71 552 85

I, I 169 183 197 210 254 ' 1 ''III' ' l' (■ ' I ' ' ''' I n/z-> 40 60 80 100 120 140 160 180 200 220 240 29.20 29.40 29.60 29,80 30,00

LB.D NP091101.M Thu Oct 18 10:43:49 2001 Page 6

NYC-WTC_00008871 1

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NYC-WTC_000088711Source: NYC Law Department, mirrored locally

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