GCMS analysis comments for sample AD28669, Dec 2001

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC04 01\28692.D Vial: 19 Acq On : 5 Dec 2001 5:56 am Operator: 209 GALOS Sample : gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Heptadecane Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 29.55 0.59 ug/1 104285 Chrysene-dl2 33.04 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Heptadecane 240 C17H36 000629-78-7 (91 2 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6 91 3 Octadecane 254 C18H38 000593-45-3 91 4 Eicosane 282 C20H42 000112-95-8 90 Abundance Scan 2669 (29.548 min): 28692.D (-) m/z 57.00 100.00% 57 43 71

5000 85

1 ■ l ’ 29.20 29.40 29.60 29.80

m/z-> — 40 60 + 118127141154 169183 80 100 120 140 160 180 200 220 240 T‘ T TT 260 280 300 m/z 43.00 69.18% Abundance #71193: Heptadecane 57

5000 71 85 1 1 I 1 ' WA. 29.20 29.40 29.60 29.80 m/z71.05 68.68% .99 ‘‘II J _i . 1.2.141 155 169 . 210 240 TTT ' ’ ir' 111 1 1 1 ' i 11 ■ ■ 1 11 1 ■' I '' ' ' i ■ ■1 11 1 1111111' 11111111111111111 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #42196: Heptadecane, 2,6,10,15-tetramethyl- 57 71 m T 1 TTI—3TTi 29.20 29.40 29.60 29.80 5000 85 m/z 85.05 41.46%

• । ' I ‘ ' T-p-r + X 113127 141 155 ■ ■ 183 ■ 1211 .......... 296 mz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #71560: Octadecane Tdrf 1 1 t ' ' 43 57 29.20 29.40 29.60 29.80 m/z 41.05 27.95% 71 5000 85

99 — J 113 127141 169183197210 254 ■ ■ r ■ i । i i r > । > । > > । > । « । । > >* । > | T i ■ « । । i i ■ ■ i T T" 1 1 1 1 • i । । ■ ' ' ' I 1 m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

28692.D GCMS1126.M Thu Dec 06 12:39:27 2001 Page 2

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