GCMS analysis comments for sample AD28677, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC0401\28677.D Vial: 13 Acq On : 5 Dec 2001 12:05 am Operator: 209 GALOS Sample : gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Heptadecane Concentration Rank 14

R.T. EstConc Area Relative to ISTD R.T.

34.54 0.86 ug/l 186732 Chrysene-dl2 33.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptadecane 240 C17H36 000629-78-7 3 2 Heneicosane 296 C21H44 000629-94-7 3 Pentacosane 352 C25H52 000629-99-2 91 4 Tetratetracontane 619 C44H90 007098-22-8 91 Abundance 57 Scan 3213 (34.538 min): 28677.D (-) m/ z 57.00 100.00% 43 71 85 5000 ----- 99 34.20 34.40 34.60 34.80 1. I _ Ji, 113 127 141 155P r169i . 183 197 "T TTr. TTTTTTTTT , 211» I I I I I 11240। I' i'l256I I r I I281 .'l . । I'I I II I I m/z 43.00 69.00% miz-> 40 I60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #71194: Heptadecane 43 57

71 5000 -========== 85 34.20 34.40 34.60 34.80 m/z 71.0,0 68.77% _ 99 113 127 141 155169183 212 240 T’ITTfuuu’u—uunuumuTKueuwuniir i h i v p r i p < i > ■ । ■ । ■ । p i m । . m/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #42201; Heneicosane i 57 71 — n।r 4 — — i 85 34.20 34.40 34.60 34.80 m/ z 51.45%

I 5000 85.05 99 113 127 141 155 268 296 ■' ■ i' ■ —TTT m/z—2 40 60 " ao" i6o 120 140 .160 180 200 220 240 260' 280 300 Abundance #73718: Pentacosane TITTr ' I 1 r ■ ■ i ■ ■ ■ ■ i ■ ' TTf 43 57 34.20 34.40 34.60 34.80 m/z 41.05 27.90% 71 5000 85

.. 1 ., 1 . 113 127 141 155/ 189 183 197 211 . .............. m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 34.20 34.40 34.60 34.80

28677.D GCMS1126.M Fri Dec 07 15:12:25 2001 Page 9

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