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GC/MS analysis results for sample AD22655, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22655 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087326–000087348

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2801\22655.D Vial: 14 Acq On : 29 Sep 2001 1:11 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Heptadecane Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

34.64 0.65 ug/1 94452 Chrysene-dl2 33.16

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heptadecane 240 C17H36 000629-78-7 93< 2 Tetracosane 338 C24H50 000646-31-1 91\ 3 Heneicosane 296 C21H44 000629-94-7 91 ) 4 Dotriacontane 451 C32H66 000544-85-4 9y^ ‘Abundance Scan 3224 (34.639 min): 22655.D (-) m/z 57.00 100.00% 57 71 43 5000 85

I 99 njLjvJ-ryl 240 256 r _____ 34.40 34.60 34.80 35.00 m/z 71.1,0 69.83% 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #32063: Heptadecane 57 71 85 5000 i 34.40 34.60 34.80 35.00 j 99 m/z 43.05 62.14% '' I ''' " I ' m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 57 71 34.40 34.60 34.80 35.00 5000- 85 m/z 85.0„0 45.07% 99 ^1^127 155169183197 294 338 ' I' ' ' ' I ' ' ‘ • I ' ' ’ ' I ‘ ' I ' ' ' ' I ' I'''' I' ni/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 -Abundance #42201: Heneicosane —/7T I'Y'i I .Ir'l I I*. In 1 I 34.40 34.60 34.80 35.00 71 m/z 55.0,0 24.01% 85 5000

99

34 J TTi^iiss 268 296 111111111111 ' I ‘ ' I'''' I''' • I I ‘ ' I ' ' '' I ■p’ ITl/Z--> 40 6080 100 120 140 160 180 200 220 240 260 280 300 320 340 34.40 34.60 34.80 35.00

22655.D NP091101.M Wed Oct 10 14:46:38 2001 Page 11

NYC-WTC_000087343

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NYC-WTC_000087343Source: NYC Law Department, mirrored locally

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