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GC/MS analysis results for sample AD22655, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22655 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087326–000087348

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\SEP2 801\22655.D Vial: 14 Acq On : 29 Sep 2001 1:11 am Operator: 209 GALOS Sample : gc/ms unknown , Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Octadecane Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

35.53 0.75 ug/1 98144 Perylene-dl2 37.28

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecane 254 C18H38 000593-45-3 91\ 2 Nonadecane 268 C19H40 000629-92-5 91 y 3 Pentacosane 352 C25H52 000629-99-2 91/ 4 Heptadecane, 9-octyl- 352 C25H52 007225-64-1 91/ Abundance Scan 3321 (35.529 min): 22655.D (-) m/z” 5?". 95”” 100.00% 57 71 43 85 5000

m/z->___ J 40 60 80 100 120 140 155 168 183 160 180 209 200 220 240 253 267 260 35.20 35.40 35.60 35.80 m/z 71.00 77.20% i^undance #71561: Octadecane I 57 43 71 85 5000 35.20 35.40 35.60 35.80 99 m/ Z ^3-0,5 68.69%

m/z-> Abundance

5000 40

43 60 57 71 80

85 ."I, . . 224 1OO_-J2Q_YL4L_J6O_[8O_JOO_2^^ #37469: Nonadecane 254

1 r-r-p—r-r-r-j- 35.20 35.40 35.60 35.80 m/z 85.05 59.28%

99 ■I ....... iy. .1??.......... m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 Abundance #73718: Pentacosane 4)3 5,7 35.20 35.40 35.60 35.80 m/z 55.00 27.26% 71 5000 85

, |ll , . I II., i| T T 40 60 80 100 120 140 160 180 200 220 240 260 35,20 35.40 35,60 35J0

22655.D NP091101.M Wed Oct 10 14:46:43 2001 Page 12

NYC-WTC_000087344

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