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GC/MS analysis results for sample AD23473, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23473 conducted on October 19, 2001.

NYC-WTC_000088725–000088752

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088748
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT1601\23473.D Vial: 4 Acq On : 16 Oct 2001 5:10 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 17 Octadecane Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 38.37 0.96 ug/1 97109 Perylene-dl2 37.23 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Octadecane 254 C18H38 000593-45-3 91\ 2 Tetratriacontane 479 C34H70 014167-59-0 91 ? 3 Heptacosane 380 C27H56 000593-49-7 91 / 4 Heptadecane 240 C17H36 000629-78-7 91' Abundance Scan 3631 (38.372 min): 23473.D (-) Tm/z 57.00 100.00% 57

85 5000

TiZz-> ^bundance u. I I I I»’I I I I I I»I I I I I I••jI»I I I I I I I Jri I I I I I I I I I I I I I I I iI I I I I I I I I I ■ I I I I I I I I I I I I I I I I I I I I I I I I I I

40 60 80 100120140 160180 200 220 240 260 280 300 320 340 360 380 400 #71561: Octadecane 38.00 38.20 38.40 38.60 38.80 m/z 71.00 74.99%

57

85 5000 38 00 38.20 38.40 38.60 38.80 m/z 43700 64.51% j224 I' <" I" " I" ‘' I" " r * •' 1 TlZz-> 40 60 80 100120140 160180 200 220 240 260 280 300 320 340 360 380 400 Abundance #58265: Tetratriacontane - 57’

38 00 38.20 38.40 38.60 38.80 5000 85 m/z 85.05 54.32%

TTfe-> ^bundance 40 60 80 100120140 160180 200 220 240 260 280 300 320 340 360 380 400

5(7- #52248: Heptacosane 311 ■367 410 1 " I » , I I I I I I . I I I H . I j

fih~yy~y^ri V y, 38.00 38.20" 38.40 38.60 38.80 “m/z STTOO^ 23.79% 553 85

281 324 380 ■m-p-rr " f"'' I' ‘" I "'' I" " I" " I ‘' I' "' I n/z-> 40 60 80 100120140160180 200 220 240 260 280 300 320 340 360 380 400 38.00 38.20 38.40 38.60 38.80

23473.D NP091101.M Wed Oct 17 13:17:57 2001 Page 17

NYC-WTC_000088748

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NYC-WTC_000088748Source: NYC Law Department, mirrored locally

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