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GC/MS analysis results for sample AD22655, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22655 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087326–000087348

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2801\22655.D Vial: 14 Acq On : 29 Sep 2001 1:11 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Docosane Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

36.39 0.41 ug/1 53030 Perylene-dl2 37.28

Hit# of 5 Tentative ID MW MolForm CAS# Qua!

1 Docosane 310 C22H46 000629-97-0 87< 2 Heptacosane 380 C27H56 000593-49-7 87\ 3 Tetratriacontane 479 C34H70 014167-59-0 87 4 Nonadecane 268 C19H40 000629-92-5 83 Abundance Scan 3415 (36.392 min): 22655.D (-) m/z 57.0,0 100.00% 57

5000 85

I m/z~> Abundance iUw , UI 169 193 265 TT.^T-rrTTT^ p"‘i 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 #44318: Docosane Trrrrp-rrq- 36.00 36.20 36.40 36.60 36.80 m/z 71.0,5 68.57%

57

85 5000 36.00 36.20 36.40 36.60 36.80 113

m/2-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 ^0 360 380 400 ' Abundance #52248: Heptacosane 57

36.00 36.20 36.40 36.60 36.80 5000 I 85 m/z 85.05 47.73%

.............. f 169 196 ^224 281 324 380 ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #58265: Tetratriacontane I . I I . -J V , , « I . . I 5(7 36.00 36.20 36.40 36.60 36.80 m/z 55,00 32,40% 5000 85

•n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 36.00 36.20 36.40 36.60 36.80

22655.D NP091101.M Wed Oct 10 14:46:48 2001 Page 13

NYC-WTC_000087345

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NYC-WTC_000087345Source: NYC Law Department, mirrored locally

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