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GC/MS analysis results for sample AD23322, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23322 conducted on October 15, 2001.

NYC-WTC_000088263–000088289

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088276
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23322.D Vial: 15 Acq On : 12 Oct 2001 3:48 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Docosane Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 29.62 1.40 ug/1 146450 Chrysene-dl2 33.12 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Docosane 310 C22H46 000629-97-0 93 2 Eicosane 282 C20H42 000112-95-8 91 3 Heptadecane 240 C17H36 000629-78-7 91 4 Tetradecane 198 C14H30 000629-59-4 91 Abundance Scan 2678 (29.623 min): 23322.D (-) m/z 56.95 100.00%. 57 43 71 5000 85

I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' 99

■n/z-> 40 uuu 60 80 .1. iJ \P1F 141154 169183 207 100 120 140 160 180 200 220 240 260 280 300 I ‘' I 310 I'' ’' I' ’' ‘ I 29.20 29.40 29.60 29.80 30.00 “mTz 43.00 68.29% Abundance #72997; Docosane 3 57

5000 71 85 JIA A 29.20 29.40 29.60 29.80 30.00 m/z 71.00 67.84% A ■nfe~> 40 uu 60 80 ^1^1^127 155169183197211

100 120 140 160 180 200 220 240 260 280 300 292 310 pT' ' I ' ' ' ' I ' ' ' ' I A

^bundance #72326; Eicosane 57 43 Ju I ' ' ' ' I 71 29.20 29,40 29.60 29.80 30.00 5000 m/z .85.05 44.34% 85 J ft 99 J ip 127141 155169 282

uL\ 'I' •' ' I ' ' I ' I I I I 11 11 '■ I ■n^-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #71193: Heptadecane 5(7 29.20 29.40 29.60 29.80 30.00 Wz 41.05 27.49%

Toi 71 85 1 99 __i J 210 141 155169 240 .......... I ' ' '' I ‘' 11''' I''' ' r '' ' I''''' I''''' I ' t' I'''' I'''' r *'' I I 1 ' ' T,/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80 30.00

23322.D NP091101.M Mon Oct 15 10:26:01 2001 Page 7

NYC-WTC_000088276

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NYC-WTC_000088276Source: NYC Law Department, mirrored locally

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