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GC/MS analysis results for sample AD23836, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23836 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089418–000089445

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089432
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3001\23836.D Vial: 16 Acq On : 31 Oct 2001 5:09 am Operator: 209 GALOS Sample ; gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peak Number 8 Docosane Concentration Rank 12 R.T. EstConc Area Relative to ISTD R.T. 29.57 1.23 ug/1 191558 Chrysene-dl2 33.06 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Docosane 310 C22H46 000629-97-0 (95 7 2 Heneicosane 296 C21H44 000629-94-7 91 3 Heptadecane 240 C17H36 000629-78-7 91 4 Eicosane ____________________ 282 C20H42 000112-95-8 91 Abundance Scan 2672 (29,570 min); 23836,D (-) mZz 56795 100.00% 57

43 71 5000 85

...... . I „l, I kl 113 J ’’27141 155169183197211225239 310 29 20 29,40 29,60 29,80 30,00 I Hl»l !■ |4>, I i4r I i-k I I f I I p I' I I |-| I I f p I ■! I p' I I I p I I I P I ' ‘ I''' ’ r^’^ '' I m/z 43705 65.13% T.fe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #44318; Docosane

lLa 71 85 253 29.20 29,40 29.60 29,80 30,00 99 4X0 m/z 71.00 63.85% 266 310 I I.11 I I I I . 11 I I . I . I I I 1 1 . J .... I , , TT-p-TT-rpTT-xyTT-rT-j-rT-rT-p-T-rT-^^ n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #42201: Heneicosane

71 85 29 20 29,40 29,60 29,80 30,00 5000 in/z^ 85.00 46.88% 99

T-q-r-r ' 'I ' ' T ' P • ■ ' ( ■ ■ ■ > p ' ■ ■ p ■ ' ' p ' ' > p ' ' ' p ' ' ' p > ■ ' p ' I I p • > ■ I Ti/z-> Abundance. 40 60 57 - 80 100 120 140 160 180 200 220 240 260 280 300 #32063; Heptadecane JUZ’ 29.20 29.40 ' 29.60 "29.80" 30.00 --m/z - 41.05 28.24% 85 5000

99 196 ' I ‘’ * I ' ' ' ' I' 240 -rfm p > ' ' p I ' I I ==^^pr=f=jX^^ ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29,20 29,40 29,60 29,80 30,00

23836.D NP103001.M Thu Nov 01 13:27:12 2001 Page 8

NYC-WTC_000089432

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NYC-WTC_000089432Source: NYC Law Department, mirrored locally

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