GCMS analysis results for sample AD28471, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC0401\28471.D vial: 7 Acq On : 4 Dec 2001 6:13 pm Operators 209 GALOS Sample : gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Docosane Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 29.55 0.92 ug/1 241390 Chrysene-dl2 33.04 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Docosane 310 C22H46 000629-97-0 93 2 Octadecane 254 C18H38 000593-45-3 91 3 Heneicosane 296 C21H44 000629-94-7 91 4 Eicosane 282 C20H42 000112-95-8 91 Abundance Scan 2669 (29.548 min): 28471 .D (-) m/z 57.00 100.00% 57 43 71 l 5000 85

99 ■ ■ i • 29.20 29.40 29.60 29.80 ■. i . A . Ji. 4 — . 14197169183197211 —........ 319 m/z 43.05 77.29% m/z-> Abundance _40 60 80 100 120 140 160 180 200 220 240 260 280 300

43 57 #72997: Docosane A 5000 71 85 WA..... 29.20 29.40 29.60 29.80 m/z 71.00 74.82% HH 100 120 140 160 180 200 220 240 260 280292300310

L 99 113 127 155169183197211 miz-> _ 40__ 60 80 Abundance #71561: Octadecane 57 43 71 i ■ ■ l ' ' 29.20 29.40 29.60 29.80 1 ’ l '

85 5000 "2 85.05 46.11%

99 _

m/z-> •11 ■ • 40 60 80 1113 127141 155.......... 224 254 ''I 1,11 I 1 ' ' I 1 1 ' ' 1 ‘1'' I ' ' ' 1 1 M M I ' ' ' * I ' ' 1 1 1 1 1 100 120 140 160 180 200 220 240 260 280 300 • • i • ‘ |

Abundance #42201: Heneicosane T - - 57 29.20 29.40 29.60 29.80 71 m/z 41.05 31.60% 85 5000 .

99 | 113 127141 155 m/z-> 4 ' " 268 296 ■ ■ ■ i ■ ■ ■

40 60 80 100 120 140 160 180 200 220 240 260 280 300 । ' i ' ■ ‘ 11031111101117 . ■■ 11 । - - — । .... 1 . 29,20 29,40 29,60 29.80

28471.D GCMS1126.M Wed Dec 05 11:27:31 2001 Page 2

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