GCMS analysis comments for sample AD28663, Dec 2001

NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\1\DATA\DEC04 01\28663.D vial: 17 Acq On 5 Dec 2001 3:59 am Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1*00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Docosane Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 29.55 1.04 ug/1 206427 Chrysene-dl2 33.04 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Docosane 310 C22H46 000629-97-0 93 2 Heneicosane 296 C21H44 000629-94-7 91 3 Nonadecane 268 C19H40 000629-92-5 91 4 Eicosane 282 C20H42 000112-95-8 91 Abundance Scan 2670 (29.552 min): 28663.D (-) m/z 57.00 100.00% 57 43 71 5000

Ju 85

99 .......................... ........................................................................................ ... .. L... 29.20 29.40 29.60 29.80 m/z43.00 70.97% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #72997: Docosane 43 57

5000 71 85 .. LA.... 29.20 29.40 29.60 29.80 m/z71.05 64.26% — 99 113127 155169183197211 292 310 T T ■ i' ■ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #42201: Heneicosane 57 U.A I I I I I I 71 ■ i ■ ■

85 29.20 29.40 29.60 29.80 5000 m/z 85.00 45.68% 99

■ ■ i ■ ■ T‘ JU 1127141 155 Ti i T i | i । 268 296 । । । । । . p-rrrp-TTITIrrrI m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #71949: Nonadecane TI" ' I' TIf 57 29.20 29.40 29.60 29.80 m/z41.00 31.30% 71 5000 85

99 J 113127 141 155 169 183 224 268 '' i ■' ITT TTm—mmu—uuutuuu"Omuuuuumuugrron m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

28663.D GCMS1126.M Thu Dec 06 15:31:25 2001 Page 2

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