GCMS analysis comments for sample AD28663, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\DEC0401\28663.D Vial: 17 Acq On 5 Dec 2001 3:59 am Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Butyl hexadecanoate Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 29.44 6.24 ug/1 1238830 Chrysene-dl2 33.04 Hit# of 5 entative ID MW MolForm CAS# Qual 1 Butyl hexadecanoate 312 C20H40O21 000000-00-0 68 2 Oxirane, /2,3-bis(1-methylethyl)-, t 128 C8H160 054644-32-5 32 3 1-Hexene, 2-methyl- 98 C7H14 006094-02-6 27 4 Cycloheptylamine 113 C7H15N 005452-35-7 27 Abundance Scan 2658 (29.442 min): 28663.D (-) m/z 56.00 100.00%

5000 41 73 257 129 T T

mz-> ■■ •i • 20 mr 40 Luz] 60 711115/ TTT 143157171185199213 239

—283. 312 80 100 120 140 160 180 200 220 240 260 280 300 m/z 29.20 29.40 29.60 29.80 57.00 47.17%

Abundance #44549: Butyl hexadecanoate

5000 258 ■ ■ i ■ • —A 29.20 29.40 29.60 29.80 73 240 312 m/z 43.05 39.04%

mz—> Abundance " ■ i " '' i' 20 40 XU 101.. 157171185 214 M. 60 129

....... I.... I. T‘‘‘11‘T 80 100 120 140 160 180 200 220 240 260 280 300 TB

#5067: Oxirane, 2,3-bis(1 -methylethyl)-, trans- 55 41 29.20 29.40 29.60 29.80 5000 m/z 41.00 37.81%

• • ■ । ■ T T IM 'I T T mz—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #63261: 1-Hexene, 2-methyl- ■ ' I ■ ' 1 'T1 1 “ 1 ' 55 29.20 29.40 29.60 29.80 m/z 55.00 30.02% 41 5000 27 70

m/z—> 20 40 60 I 98 80 100 120 140 60 180 200 220 240 260 280 300 ' ..... AAA 29.20 29.40 29.60 29.80

28663.D GCMS1126.M Thu Dec 06 15:31:23 2001 Page 1

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