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GC/MS analysis results for sample AD23839, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23839 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089366–000089384

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089376
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File ; C:\HPCHEM\1\DATA\OCT3001\23839.D Vial: 13 Acq On : 31 Oct 2001 2:14 am Operator; 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title ; 209 625/TCLP calibration table Library ; C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Butyl hexadecanoate Concentration Rank 1,

R.T. EstConc Area Relative to ISTD R.T. 29.45 1.21 ug/1 291219 Chrysene-dl2 33.06 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Butyl hexa^Jecanoate 312 C20H40O2i 000000-00-0 35 2 Oxirane, ,3-bis(l-methylethyl)t 128 C8H16O 054644-32-5 32 3 1-Hexen^ , 2-methyl- 98 C7H14 006094-02-6 27 ■ 4 4-Dec lie, 2-methyl-, (E) - 154 C11H22. 028665-56-7 16 Abundance/ Scan 2659 (29.452 min): 23839.D (-) m/z 56.00 100.00% 53

5000 41 257 312 29.20 29.40 29.60 29.80 m/z 57.00 47.42% TiZz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #44549: Butyl hexadecanoate 5

,,,,,, ,.P,.,/, 5000- 258 29.20 29.40 29.60 29.80 240 312 TTpz 41705 34.74% 7 ^29 f''''I''''I ''' r I • ■' I (•‘ ' I ■■■ ■ I'''' I'''' I I'''' I' ' I TiZz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5067: Oxirane, 2.3-bis(1-methylethyl)-, trans- 53

41 29.20 29,40 29.60 29.80 5000 m/z 43.05 34.55%

I J VTTYy-rT'-T-Tq--t-rn-T-y-rTnrTyT-rT--r^^^ Tife-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 'Kbundance - #1354:1-Hexene, 2-methyl- - 29.20 .29.40 29.60-29.80— Wz 55.00 29.97% 41 5000

27 70 Il 98 .. , ..... tt/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

23839.D NP103001.M Thu Nov 01 14:35:57 2001 Page 4

NYC-WTC_000089376

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NYC-WTC_000089376Source: NYC Law Department, mirrored locally

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