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GC/MS analysis report for sample AD22546, September 2001

Machine-extracted title · confidence 95%

Laboratory results for sample AD22546 indicating other unknown compounds detected via GC/MS on September 27, 2001.

NYC-WTC_000086949–000086971

Folder label: “508 Scan 9/17/01 9/26/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C;\HPCHEM\l\DATA\SEP2501\22546.D Vial: 12 Acq On : 26 Sep 2001 1:14 am Operator: 209 GALOS Sample : GC/MS unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Butyl hexadecanoate Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T, 29.53 1.43 ug/1 218760 Chrysene-dl2 33.16 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Butyl hexad@<fanoate 312 C20H40O2 000000-00-0 53 2 Oxirane, ,3-bis(1-methylethyl)t 128 C8H16O 054644-32-5 32 3 1-Hexe^ , 2-methyl- 98 C7H14 006094-02-6 27 4 2-De, ne, 9-methyl-, (Z)-_________ 154 C11H22 074630-24-3 25 ^bundanceZ Scan 2668 (29.534 min); 22546.D (-) m/z 56.00 100.00% 53

5000 4' 73 129 257 29.20 29.40 29.60 29.80 312 T-nrrn-ri-rr in/z sYToy 4^795% •n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #44549: Butyl hexadecanoate 5

5000 258 29.20 29.40 29.60 29.80 240 312 129 m/z 43.05 38.23% 101 I 157171185 214 ....../..I.... I' ' ''I' T Tlfe~> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5067: Oxirane, 2,3-bis(1-methylethyl)-, trans- 5 41 1 ,-rt 29.20 29.40 29.60 29.80 5000 m/z 41.05 36.52% 73 J 113128 Ti/z-> 20 40 60 80 100 120 140 160 180 200 . 220 240 260 280 300 ^bundance #1354; 1-Hexene, 2-methyl- 53 29.20 29.40 29.60 29.80 m/z 73700 31.66% 41 5000

27 I 70

n/z~> p 20 XUu 40 60 80 98 I'''' I'''' I'''' I'''' I'''' I'''' I' ‘' I'''' I ‘‘ I'''' I 100 120 140 160 180 200 220 240 260 280 300 ' ' 1 2^20 29.40 29.60 29.80

22546.D NP091101.M Wed Oct 03 14:44:33 2001 Page 5 NYC-WTC_000086961

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NYC-WTC_000086961Source: NYC Law Department, mirrored locally

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