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GC/MS analysis report for sample AD22546, September 2001

Machine-extracted title · confidence 95%

Laboratory results for sample AD22546 indicating other unknown compounds detected via GC/MS on September 27, 2001.

NYC-WTC_000086949–000086971

Folder label: “508 Scan 9/17/01 9/26/01

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Scanned page image, NYC-WTC_000086962
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2501\22546.D Vial: 12 Acq On : 26 Sep 2001 1:14 am Operator: 209 GALOS Sample : GC/MS unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Tricosane Concentration Rank 11 R.T. EstConc Area Relative to ISTD R.T. 30.73 0.58 ug/1 89561 Chrysene-dl2 33.16 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Tricosane 324 C23H48 000638-67-5 91 2 Eicosane 282 C20H42 000112-95-8 91 3 Heptadecane 240 C17H36 000629-78-7 90 4 Octadecane ___________________________ 254 C18H38 000593-45-3 90 Abundance Scan 2798 (30.727 min); 22546.0 (-) m/z 57.00 100.00%

43 71

5000 85

Ti/z-> 40 JLU 60 ,1 197 Y’lS-T^’YT'TTTjT'VrTYTT-rTyT-rT-^^ I'''' I 281 80 100 120 140 160 180 200 220 240 260 280 300 320 30.40 30.60 30.80 31.00 in/z 71.00 71.98% Abundance #73318: Tricosane 3 57

71 5000 85 I ' ' y.4O 30.60 30.80 31.00 m/z 43.05 67.79% I I 113127141 183197211225 296 324 I'''' I'''' I'''' I T 11' •' 111'' I ■ •' 1111' n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #72323; Eicosane 43 30.40 30.60 30.80 31.00 71 5000 m/z 85.05 46.97% 85

^1^ 113127141 282 ■Q i'''' I'''' I'''' I'''' I'''' I'''' I'''' I T-p-r-r-rp-n-rp ■nZz-> Abundance 40 60

5|7 80 100 120 140 160 180 200 220 240 260 280 300 320 #71193: Heptadecane l\ ' I y.4O 30.60 30.80 31.00 m/z 41.05 25704% 5000 71 ft 85

99 xrpUrJr , J ^^^127141155169 210 240 ' I"' ' ' I '' I' I' ' I ' I''''' I''' ' I'' ' ' I' ''' I ' ''' I''' ' I'''' I'''' r ''' r ' ■n/z~> .40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 30.40 30.60 30.80 31.00

22546.D NP091101.M Wed Oct 03 14:44:35 2001 Page 6

NYC-WTC_000086962

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NYC-WTC_000086962Source: NYC Law Department, mirrored locally

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