GCMS analysis comments for sample AD28677, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC04 01\28677.D Vial: 13 Acq On 5 Dec 2001 12:05 am Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Tricosane Concentration Rank 13

R.T. EstConc Area Relative to ISTD R.T.

30.63 0.89 ug/1 194554 Chrysene-dl2 33.03

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tricosane 324 C23H48 000638-67-5 2 Hexatriacontane 507 C36H74 000630-06-8 3 Eicosane 282 C20H42 000112-95-8 91 4 Tetracosane 338 C24H50 000646-31-1 90 Abundance Scan 2787 (30.627 min): 28677.D (-) m/ z 57.0.0 100.00% 57 43 71 5000 85 — — — — 99 , 30.20 30.40 30.60 30.80 31.00

m/z-> ..401,4.60__A,804,4,14127 141155169183197210 ........ . ........ . 100 120 140 160 180 200 220 240 260 280 300 320 m/z 43.00 69.40% Abundance #46165: tricosane 1 43 57

71 5000 85 30.20 30.40 30.60 30.80 31.00 m/z 71.00 6 6.34% 99 113127 155169183197211 253 297 324 — III I I n •' TT । *■ ‘II I ’ ' ' • I i11 111' '1 • i TTTTITTTTTTT miz-2 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #74636: Hexatriacontane 4.3 57 — 71 30.20 30.40 30.60 30.80 31.00 5000 85 m/z 85.0 45.23%

I QQ ... L.... _ 11127141155 169 183 197211 ........................... miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #39862: Eicosane 43 57 30.20 30.40 30.60 30.80 31.00 71 m/z 41.05 32.96% 5000 85

99 113127 141 155 196 TT .. f, । TT ,. ।, TT । TPTTIT 11111 240 282 -==-4====-=PPPP4=P=== 111 ■1 ■111 I ■ ■ i ■ T ’ I “1'' I'''' I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 30.20 30.40 30.60 30.80 31.00

28677.D GCMS1126.M Fri Dec 07 15:12:00 2001 Page 4

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