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GC/MS analysis report for sample AD22493, September 2001

Machine-extracted title · confidence 95%

Laboratory results for sample AD22493 indicating other unknown compounds detected via GC/MS on September 27, 2001.

NYC-WTC_000086827–000086851

Folder label: “508 Scan 9/15/01 9/26/01

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Scanned page image, NYC-WTC_000086836
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2501\22493.D Vial: 4 Acq On : 25 Sep 2001 5:22 pm Operator: 209 GALOS Sample : GC/MS unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Tricosane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T.

30.73 2.21 ug/1 259924 Chrysene-dl2 33.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

Tpgosane 324 C23H48 000638-67-5 93 iQc t a^ecane' 254 C18H38 000593-45-3 91 HepEadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6 91 4 Tetracosane 338 C24H50 000646-31-1 90 Abundance Scan 2798 (30.731 min): 22493.D (-) m/z 56795 100.00% 57 43 71

5000 85

T 30.40 30.60 30.80 731.00 njlvJl-ryi 324 m/z 71.10 H2.29% tVz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #73318: Tricosane 43 57

71 5000 85 30.40 30.60 30.80 m/z 43.00 \£7.19% Il II 183197211225 324 296 '' I''' A — nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #71561: Octadecane 57 43 71 " ' ' I 30.40 30.60 30.80 31.00 85 m/z 85.05 49.76% 5000

w 99 I 113127141155 224.... 254 V ■ I'' I '^r rp-m-pn-r^ ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 ^bundance #42196: Heptadecane, 2,6,10.15-tetramethyl- 57 30.40 30.60 30.80 31.00 71 m/z 41705 25.05%

5000 85

T 183 211 I ' I'''' I ’''' I ’ 268 296 p-n-rp-n-rp T^YTT44pVrpH-T-Tpn-rTny‘rnnTyrTYp-TTT^ ’ 'I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 30.40 30.60 30.80 31.00

22493.D NP091101.M Wed Sep 26 11:36:39 2001 Page 2 NYC-WTC_000086836

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NYC-WTC_000086836Source: NYC Law Department, mirrored locally

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