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GC/MS analysis results for sample AD22655, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22655 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087326–000087348

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087341
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\SEP28O1\22655.D Vial: 14 Acq On : 29 Sep 2001 1:11 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Tricosane Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

32.77 0.74 ug/1 108014 Chrysene-dl2 33.16

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tricosane 324 C23H48 000638-67-5 91. 2 Dotriacontane 451 C32H66 000544-85-4 91' 3 Pentacosane 352 C25H52 000629-99-2 91 4 Heptadecane 240 C17H36 000629-78-7 91z f^bundance Scan 3020 (32.766 min): 22655.D (-) m/z ■57.0.0 100. ‘00% 57 I

i1 5000 85

32.40 32.60 32.80 33.00

-n/z-> JjUXX. 100 150 183 207 200 250 300 350 400 450 m/z 71.1.0 74.95% Abundance #73318: Tricosane 40 71 ■ I I ■ ■ I ■ I 1 ' /■ I r*. I I"! I rrt । f 5000 32.40 32.60 32.80 33.00 m/z 43.00 68.15% I I 127 183 211 .... 296 324 .............. Wz->_____ 50 100 150 200 250 300 350 400 450 Abundance #74490: Dotriacontane 43 .

. 71 32.40 32.60 32.80 33.00 5000 m/z 85.0,5 50.47%

127 155 183 379 407 450 Tl/2-> i\bundance 50

43 100 150 200 250 300 #73718; Pentacosane 350 400 450 J] 32.40 32.60 32.80 33.00 m/z 41.05 28.59% 71 A 5000

m/z-> MJ 50 , 127 155 -183 211............................................................................... 100 ' ' 150 200 25o' 300 35o' ' '460 45o' 32.40 32.60 32.80 33.00

22655.D NP091101.M Wed Oct 10 14:46:29 2001 Page 9

NYC-WTC_000087341

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