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GC/MS analysis results for sample AD22655, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22655 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087326–000087348

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2801\22655.D Vial: 14 Acq On : 29 Sep 2001 1:11 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 10 Pentacosane Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

33.72 0.96 ug/1 140676 Chrysene-dl2 33.16

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pentacosane 352 C25H52 000629-99-2 91 2 Heptadecane 240 C17H36 000629-78-7 91 3 Tetracosane 338 C24H50 000646-31-1 90 4 Eicosane 282 C20H42 Abundance Scan 3”l"24 (33.721 min)? 22655.D (-j 5—OP- 0112-95-8 . 90 4’’ 71 43 85 5000

,, .1 , Ji , j , |J|,, 69183197211 227 253 ,281 33.40 33.60 33.80 34.00 T-r-p-r m/z 71.00 73.59% m/z->___ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ’Abundance #73718: Pentacosane 4|3 5.7

71 r/ , . rp. rv.-p 5000 85 33.40 33.60 33.80 34.00 m/z 43.0,5 61.13% j J- ‘♦■’155169183197211225 I'''' I m/2-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ^Abundance #71193: Heptadecane 57

71 33.40 33.60 33.80 34.00 5000 85 m/z 85.05 52.39% 99 ’♦^127141155169 210 240 X^-rTTYrrTTYrri-rp-rTTYrr'^ I ' ' • ' I ' ' ' ' I ' ' T ■n m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane T I ' ' ' ' I ' ' ' ' I 43 517 33.40 33.60 33.80 34.00 71 m/z 55.00 22.21% 5000 85

99 iio □ J l| ' I ‘ ' I ' ' ' 155169183197 294 338 Tl/Z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 33.40 33.60 33.80 34.00

22655.D NP091101.M Wed Oct 10 14:46:34 2001 Page 10

NYC-WTC_000087342

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