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GC/MS analysis results for sample AD23650, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23650 conducted on October 19, 2001.

NYC-WTC_000089000–000089024

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000089019
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

-—Library—Search- Compound Report Data File ; C:\HPCHEM\1\DATA\OCT1601\23650.D Vial: 15 Acq On : 17 Oct 2001 3:56 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Pentacosane Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 34.61 1.10 ug/1 133813 Chrysene-dl2 33.13 Hit# Of 5 Tentative ID MW MolForm . CAS# Qual

1 Pentacosane 352 C25H52 000629-99-2 90^ 2 Heneicosane 296 C21H44 000629-94-7 90. 3 Tetracosane 338 C24H50 000646-31-1 90, 4 Octadecane 254 C18H38 000593-45-3 90 Abundance Scan 3221 (34.614 min); 23650.D (-) m/z 57.00 100.00%! 5|7

43 71 85 553

UI I .-r. , I , , , , I 1 99 34.20 34.40 34.60 34.80 35.00 256 ■........................................ .......

I'''' I'''' I'''' I "mTz 43705 67744% TTfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73718: Pentacosane 40 07

5000 71 85 I ^1 ZU 34.20 34.40 34,60 34.80 35.00 m/z 71.10 67.56% I" I'''' 13127141155169183197211225 I I I”' ‘' I'''' I'''' (''' I' ' I'''' I'''' I'' ‘' I I • • " I' " ' I' • *' I " " I' 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340

I ■nZz-> ^bund 3nC6 ------ - #42201 :Heneicosane 57 71 85 34.y 34.40 34.60 34.80 35.00 aSfl “inTz 85705 57716% 99

■n/z-> 40 44 ' I •' 268 296 ' r ' * ’ I''' * I'''' I' ‘' I' ‘' I 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 111 v I p-i I r| I

Abundance —— #73543:-Tetracosane—— ------- 43-57— -34.y 34.40 34.60 34:80" 35.00 71 "m/z 41.05 24.44%

553 85

[ I il 155169183197 294 338 '' I'''' 1 ‘I' ’VrylH-ri^YTTV-rpVrTp-rrVp-f-rTy^TTTYrT^^ ''' I'''' I''' 'I' 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 34.20 34.40 34.60 34.80 35.00

23650.D NP091101.M Thu Oct 18 10:40:31 2001 Page 13 NYC-WTC_0000896i9

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NYC-WTC_000089019Source: NYC Law Department, mirrored locally

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