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GC/MS analysis results for sample AD23650, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23650 conducted on October 19, 2001.

NYC-WTC_000089000–000089024

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000089020
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library -Seareh-Gompound-Report Data File : C:\HPCHEM\1\DATA\OCT1601\23650.D Vial: 15 Acq On : 17 Oct 2001 3:56 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1,00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 Tricosane Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 35.50 1.01 ug/1 106543 Perylene-dl2 37.24 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tricosane 324 C23H48 000638-67-5 91k 2 Triacontane 422 C30H62 000638-68-6 93< 3 Tetracosane 338 C24H50 000646-31-1 90 4 Nonacosane 408 C29H60 000630-03-5 90 Abundance Scan 3318 (35.504 min): 23650.D (-) m7z SYTOO 100.00% 57

85 5000

' ' ' r' ' ‘r' i' ■' T ' I 35.20 35.40 35.60.35.80 169 197 281 TyTTTTpT-rrpTTTpT-rrpTTTyrTTTp-rTTpTTTTpTrr^^ m/z 71.10 65.68% TiZz-> 40 60 80 100120140160180 200220240260280 300320340 360380 400420 Abundance #73318; Tricosane 43

5000 71 — m/z A 35.20 35.40 35.60 35.80 43.05 62.54% 1

183 211 I' ‘' i'"' '''' I 296 324 JTTTTpTTTpTTTp-n-ryr^ ft Tl/z-> 40 60 80 100120140160180200220 240260280 300320340 360380 400420 — Abundance ■ - - #55461; Triacontane 4(3

71 35.20 35.40 35.60 35.80 553 m/z 85.05 56.49%

239 267 379 422 ' " I ‘" nZz-> 40 60 80 100120140160180 200 220 240 260280 300 320340 360380 400420 Abundance———------ —#73543: Tetracosane --- ———— — 7 ' 35.20 35 40"35.60 35.80 m/z 41.05 24.17% 5000 85

294 338 yrrrr^xriyrrtTY^-rr^TTrrYrTr^ r "' r "' I I" " I" " I"' 'T'" I"'' I" " I" " I nZz-> 40 60 80 100120140160180 200220 240260280300320340 360380 400420 35.20 35.40 35.60 35.80

23650.D NP091101.M Thu Oct 18 10:40:33 2001 Page 14 NYC-WTC_06b089020“

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NYC-WTC_000089020Source: NYC Law Department, mirrored locally

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