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GC/MS analysis results for sample AD23605, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23605 conducted on October 19, 2001.

NYC-WTC_000088935–000088960

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088956
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NYC 9/11 Public Portal Document

Library Search Compoun'd Report Data File ; C:\HPCHEM\1\DATA\OCT1601\23605.D Vial: 12 Acq On ; 17 Oct 2001 1:00 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Library : C;\DATABASE\NBS75K.L ********************************* * * ************************************** Peak Number 15 Pentacosane Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 36.37 1.15 ug/1 108046 Perylene-dl2 37.23 Hit# of 5 Tentative ID MW MolForm . CAS# Qual

1 Pentacosane 352 C25H52 000629-99-2 91 2 Hexatriacontane 507 C36H74 000630-06-8 91 3 Triacontane 422 C30H62 000638-68-6 9T 4 Nonacosane ;_____ ______________ 408 C29H60 000630-03-5 90 Abundance Scan 3412 (36.366 min): 23605.D (-) m/z SYTOO 100700% 57

85 5000

3! .1, J 183 209 36.00 36.20 36.40 36.60 281 nfe-> M40 60 80 100120140160180 200220 240260280 300320340 360380 400420 m/z 71.10 70.55% Abundance #73718: Pentacosane 43

71 5000 " Ct I . I I I I .r7Y'|^?7r9 i*/ 36.00 36.20 36.40 36.60 m/z43705 67.96% I ' I . I r f. I 1 \ . I I I . . ‘i I . I . 1 I I I I I I I I I I I r "‘ I' "'I" " r ‘"I" "r"'i n/z-> 40 60 80 100120140160180 200220 240260280 300 320340 360380 400420 Abundance #74636: Hexatriacontane .57__

36.00 36.20 36.40 36.60 5000 in/z 85.05 51.97% 85

1 U 141 169 197 jTTVq+rriYTTTrpTrrpTrrVpTrrp^ pTTTpTTTyrTTTpTmrpTTr|TT-rryrrTTpTTTYrT^^ n/z-> 40 60 80 100120140160180200220 240260280300320340 360380 400420 ^bundance #55461: Triacontane 43 .^^J6W_J6,20_3640_36,60__^_ --m-Az— 55.00 24.54% 71 5000

239 267 379 422 . ... . I" " I" " I" " r "' I ‘' I"' ‘ I"' •nZz-> 40 60 80 100120 140160 180 200220 240260280 300 320340 360380 400 420 36.00 36.20 36.40 36.60

23605.D NP091101.M Thu Oct 18 10:32:52 2001 Page 15

NYC-WTC_OOO688956

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NYC-WTC_000088956Source: NYC Law Department, mirrored locally

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