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GC/MS analysis results for sample AD23080, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23080 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087817–000087841

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document

• Data File C:\HPCHEM\1\DATA\OCT0301\23080.D Vial: 7 Acq On 3 Oct 2001 6:30 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Pentacosane Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

32.76 1.26 ug/1 181734 Chrysene-dl2 33.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1’ Pentacosane 352 C25H52 000629-99-2 9K 2 Heptadecane 240 C17H36 000629-78-7 91 ^ 3 Docosane 310 C22H46 000629-97-0 90 / 4 Tetracosane 338 C24H50 000646-31-1 90/ iAbundance Scan 3019 (32.760 min): 23086.D (-) m/z 57.0.0 100 .'O6% 43 71 85 5000

ni/z-> Abundance 40 u 60 413 57 80 100 120 140 160 180 200 220 240 260 280 300 #73718: Pentacosane ■m- 32.40 32.60 32.80 33.00 m/z 71,00 70.64%

iI 5000 71 85 A r' 32.40 32.60 32.80 33.00 I ' m/z 43.05 66.43% I, Ip 127 141 155 169 183 197211 225 n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #71193: Heptadecane 57

71 32.40 32.60 32.80 33.00 5000 85 m/z 85.0.5 50.62%

99 ■ j 113 127 141 155169 210 240 I " " I' '-'-'-r- I ' ' ' ' I ' ' ' ' I [n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #44318: Docosane 7 32.40 32.60 32.80 33.00 71 m/z 25.54% 85 5000

99 J, 266 310 I ‘' '' I' ' ' 'I' ' I I ' ' ' ’ I ' ' ' ' I ' ' ' ’ •n/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 32.40 32.60 32.80 33.00

23080.D NP091101.M Tue Oct 09 10:02:11 2001 Page 11

NYC-WTC_000087834

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NYC-WTC_000087834Source: NYC Law Department, mirrored locally

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