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GC/MS analysis results for sample AD22777, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22777 conducted on October 5, 2001, identifying unknown compounds.

NYC-WTC_000087953–000087972

Folder label: “GC/MS Scan 9/21/01

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Data File : C:\HPCHEM\1\DATA\OCT0401\22777.D Vial: 8 Acq On : 4 Oct 2001 10:23 pm Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Pentacosane Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 32.76 0.66 ug/1 106917 Chrysene-dl2 33.15 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pentacosane 352 C25H52 000629-99-2 91 2 Tetracosane 338 C24H50 000646-31-1 90\ 3 Pentadecane 212 C15H32 000629-62-9 90/ 4 Heptadecane ____________________ 240 C17H36 000629-78-7 9o' Abundance Scan 3019 (32.759 min): 22777.D (-) m/z 57.00 100.00% 57 71 43 85 5000

99 32.40 32.60 32.80 33.00 'I" ’' I" I " ........................................... m/z 71.10 77.47% TiZz-> 40 60 80 100 120 14C 140 160 180 200 220 240 260 280 300 320 340 Abundance #73718: Pentacosane 43 57

71 5000 ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' 85 32.40 32.60 32,80 33.00 m/z43.05 66.93%

Tife-> 40 J60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ■ I ■ I ^^127141155169183197211225________________________

Abundance #73543: Tetracosane 43 5 7 71 32.40 32.60 32.80 33.00 5000 85 m/z85.05 53 .41%

99

•n/z~> 40 " i'' 44 60 l| '']^127 155169183197 I'''' I'''' I'' ‘' I'''' I'''' I'''' I'''' I'''' I'''' I'" ‘ I" " I'''' I' 80 100 120 140 160 180 200 220 240 260 280 300 320 340 294 338

Abundance #70278: Pentadecane A 435^ 32.40 32.60 32.80 33.00 m/z41.05 26.41% 71 5000 85

212 . 11. r 11 ri.. 1*711 '■ 1111. r ''' I' ’'' I'''' I ’''' I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 32.40 32.60 32.80 33.00

22777.D NP091101.M Fri Oct 05 12:49:18 2001 Page 7

NYC-WTC_000087966

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