NYC 9/11 Public Portal Document
' . Data File C:\HPCHEM\1\DATA\OCT0 3 01\23080.D Vial: 7
Acq On 3 Oct 2001 6:30 pm Operator: 209 GALOS
Sample gc/ms unknown Inst : GC/MS 209
Mise Multiplr: 1.00
MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator)
Title : 209 625/TCLP calibration table 7/16/01
Library : C:\DATABASE\NBS75K.L
*********************************************************************
Peak Number 13 Hexatriacontane Concentration Rank 6
R.T. EstConc Area Relative to ISTD R.T.
34.63 1.17 ug/1 168374 Chrysene-dl2 33.15
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Hexatriacontane 507 C36H74 000630-06-8 94
2 Tetracosane 338 C24H50 000646-31-1 91
3 Heneicosane 296 C21H44 000629-94-7 91
4 Pentacosane 352 C25H52 000629-99-2 91
Abundance Scan 3223 (34.632 min):'23680.0 (-) m/z 57.00 100700%
57
71
a
43
5000 85
mZz->
JJ
40
■ 1.1.4.
99
221 239 256 281
‘p-T'lTp'rTT-+YrT^lHpiVT-rp-T-rVp-rTT-p--r-rTyT-T-r-r-p*T-rp--rT-r-rp-r-rp-^
60 80 100 120 140 160 180 200 220 240 260 280 300 320 340
T-p-n-rp- m/z
34.40 34.60 34.80 35.00
71.10 68.61%
Abundance #74636: Hexalriacontane ........ ...
43 57
71
5000 85 34.40 34.60 34.80 35.00
i m/z 43.05 64.18%
l! T \1^‘'?7141155169183197211
r
m/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340
Abundance #73543: Tetracosane
43 57
: 71
34.40 34.60 34.80 35.00
5000 85 m/z 85.05 47.30%
99
:i 1J3127 155169183197
L
I I j-| -T-pn^rTq-TVrryT-r-rTjT-r-rTq-T-^^
294 338
I' ‘• I' ’'' I' " ' I'
40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340
'Abundance #42201: Heneicosane
I 7 34.40 34.60 34.80 35.00
71 m/z 41.00 25.30%
85
5000
99
tXt*. 268 296
I ' ' ' ' I ' ’ ' ' I ' ' ' ' I I'''' I''' 11'
m/Z“> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 34.40 34.60 34.80 35.00
23080.D NP091101.M Tue Oct 09 10:02:19 2001 Page 13
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NYC-WTC_000087836
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