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GC/MS analysis results for sample AD23080, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23080 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087817–000087841

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document

' . Data File C:\HPCHEM\1\DATA\OCT0 3 01\23080.D Vial: 7 Acq On 3 Oct 2001 6:30 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Hexatriacontane Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

34.63 1.17 ug/1 168374 Chrysene-dl2 33.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 94 2 Tetracosane 338 C24H50 000646-31-1 91 3 Heneicosane 296 C21H44 000629-94-7 91 4 Pentacosane 352 C25H52 000629-99-2 91 Abundance Scan 3223 (34.632 min):'23680.0 (-) m/z 57.00 100700% 57 71

a 43 5000 85

mZz-> JJ 40 ■ 1.1.4. 99 221 239 256 281 ‘p-T'lTp'rTT-+YrT^lHpiVT-rp-T-rVp-rTT-p--r-rTyT-T-r-r-p*T-rp--rT-r-rp-r-rp-^ 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 T-p-n-rp- m/z 34.40 34.60 34.80 35.00 71.10 68.61% Abundance #74636: Hexalriacontane ........ ... 43 57

71 5000 85 34.40 34.60 34.80 35.00 i m/z 43.05 64.18% l! T \1^‘'?7141155169183197211 r m/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 57 : 71 34.40 34.60 34.80 35.00 5000 85 m/z 85.05 47.30% 99 :i 1J3127 155169183197

L I I j-| -T-pn^rTq-TVrryT-r-rTjT-r-rTq-T-^^ 294 338 I' ‘• I' ’'' I' " ' I' 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 'Abundance #42201: Heneicosane I 7 34.40 34.60 34.80 35.00 71 m/z 41.00 25.30% 85 5000

99 tXt*. 268 296 I ' ' ' ' I ' ’ ' ' I ' ' ' ' I I'''' I''' 11' m/Z“> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 34.40 34.60 34.80 35.00

23080.D NP091101.M Tue Oct 09 10:02:19 2001 Page 13

! NYC-WTC_000087836

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NYC-WTC_000087836Source: NYC Law Department, mirrored locally

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