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GC/MS analysis results for sample AD23080, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23080 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087817–000087841

Folder label: “GC/MS Scan 9/21/01

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Scanned page image, NYC-WTC_000087837
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NYC 9/11 Public Portal Document

' , Data File C:\HPCHEM\1\DATA\OCT0301\23080 .D Vial: 7 Acq On 3 Oct 2001 6:30 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 Hexatriacontane Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T.

35.52 0.95 ug/1 120949 Perylene-dl2 37.28

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91. 2 Heneicosane 296 C21H44 000629-94-7 91 ) 3 Docosane 310 C22H46 000629-97-0 91 / 4 Tetracosane 338 C24H50 000646-31-1 91/ Sundance Scan‘3320 (35.523 min): 23080.0 (-) “.. ........... * m/ z 100.00%

JL 57 43 71 85 5000

99 35.20 35.40 35.60 35.80 I 209 ............... 281.......... m/z 73.15% nn/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #74636: Hexatriacontane 43 5 7 I

5000 71 85 A 35.20 35.40 35.60 35.80 m/z 43.00 70.47% I IL 1^^133 197 211 •1\T--r‘^-rYrT-Ti--fT-i-T-T-Yry-T-T-Yr-r-riyT^-^-TYr-rT-rYr-rT-TyT-T-T^^ m/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300

Ji Abundance #42201; Heneicosane 57 , 71 ' , 85 35.20 35.40 35.60 35.80 5000 m/z 85.05 53.73% 99 i 113127141155 296 268 I'''' I 'n/2-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #44318: Docosane 7 35.20 35.40 35.60 35.80 71 m/z 55.0,0 26.56% 85 5000

40 uu 60 80 99 .,40 l| J’127 141155 IM -T‘Y‘r-r-‘hq-TA-T-TqS-T-rA-yT-Vv--rpT-T-^^ 100 120 140 160 180 200 220 240 260 280 300 266 r '' ' I 310 35:20 3540 35:60 35.80

23080.D NP091101.M Tue Oct 09 10:02:24 2001 Page 14

NYC-WTC_000087837

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NYC-WTC_000087837Source: NYC Law Department, mirrored locally

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