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GC/MS analysis results for sample AD23606, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23606 conducted on October 19, 2001.

NYC-WTC_000088961–000088985

Folder label: “GC/MS Scan 9/27/01

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NYC 9/11 Public Portal Document

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Library Search Compound Report Data File ; C;\HPCHEM\1\DATA\OCT1601\23606.D Vial: 13 Acq On : 17 Oct 2001 1:59 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 Hexatriacontane Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 36.36 1.07 ug/1 113115 Perylene-dl2 37.24 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 9L 2 Heneicosane 296 C21H44 000629-94-7 91 3 Tetratetracontane 619 C44H90 • 007098-22-8 91 4 Triacontane 422 C30H62 000638-68-6 9L Abundance Scan 3412 (36.365 min): 23606.D (-) m/z 57.00 100.00% 57

85 5000

mfe-> UMW 50 100 150 1?] ... 200 281 250 300 350 400 ..... 450 500 550 .......... 600 36,00 36.20 36.40 36,60 m/z 43.05 71.21% Abundance #74636: Hexatriacontane 57

85 36,00 36,20 36,40 36,60 m/z 71.10 70.14%

' ' ' I' ■ ft 1601502602^3^" 350 4TO 450 ' ' ^0 550 ' 600 ' m/z-> 50 Abundance #42201: Heneicosane —57

85 36,00 36,20 36,40 36,60 5000- m/z 85.05 51.14%

if ,268296 , . , ............................................

mte-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #74745: Tetratetracontane - 36,00 36,20 - 36,40 - 36,60 - m/z 557 00^ ' 25-. 98% 5000 85

463491519547 591618 m/z-> 50 •100 150 200 250 300 350 400 450 500 550 600 36,00 36,20 36,40 36,60

23606.D NP091101.M Thu Oct 18 10:36:10 2001 Page 15 ■

NYC-WTC_000088982

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NYC-WTC_000088982Source: NYC Law Department, mirrored locally

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