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GC/MS analysis results for sample AD23320, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23320 conducted on October 15, 2001.

NYC-WTC_000088207–000088236

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088230
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\OCT1201\23320.D Vial: 13 Acq On : 12 Oct 2001 1:51 pm Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 17 Hexatriacontane Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 36.36 2.41 ug/1 229095 Perylene-dl2 37.22

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Heneicosane 296 C21H44 000629-94-7 91 3 Tetratetracontane 619 C44H90 007098-22-8 91 4 Tricosane 324 C23H48 000638-67-5 9T Abundance Scan 3412 (36.360 min): 23320.D (-) m/z 57.00 100.00% 57 A 85 5000- R T 36.00 36.20 36.40 36.60 , 239 m/z 71.00 78.31% ■nfe-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #74636; Hexatriacontane 57

5000- 85 36.00 36.20 36.40 36.60 m/z 43705 65.75% Jl^J^^+li^^^TR-rT-p-TT-p-T-r-rT-p-TT-p-rT^^ n-r-p ■n/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #42201: Heneicosane 57 T T V 36.00 36.20 36,40 36.60 85 5000 m/z 85.05 50.20% A 268296 n-r-p ■nfe-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #61068: Tetratetracontane p-rV-r-p 5(7 36.00 36.20 36.40 36.60 m/z55.00 21.54%

WiiBi 85

ri'* 97225 379407 590618 T-p ' I ' ' ' ■n/z-> 50 100 150 2ro 250 3(W 350 400 450 500 550 600 36.00 36.20 36.40 36.60

23320.D NP091101.M Mon Oct 15 09:54:08 2001 Page 17

NYC-WTC_000088230

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NYC-WTC_000088230Source: NYC Law Department, mirrored locally

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