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GC/MS analysis results for sample AD23320, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23320 conducted on October 15, 2001.

NYC-WTC_000088207–000088236

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088231
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NYC 9/11 Public Portal Document

■J Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23320.D vial: 13 Acq On : 12 Oct 2001 1:51 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise ■ Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 18 Hexacosane Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 37.30 1.70 ug/1 161251 Perylene-dl2 37.22 Hit# of 5 Tentative ID MW MolForm CAS# Qual C)Hexacosane 366 C26H54 000630-01-3 80 2 Docosane 310 C22H46 000629-97-0 72 3 Heptadecane, 9-octyl- 352 C25H52 007225-64-1 72 4 Eicosane, 10-methyl- 296 C21H44 054833-23-7 .72 Abundance Scan 3514 (37.296 min): 23320.D (-) m/z SYTOO 100.00% 57

85 5000 4' 11Q Jl it ,In- 209225 267 37.00 37.20 37.40 37.60 r* ,'i r.. i"|,,7,1,,:. f.,,, I,, I,,,, I, 11 ,, I I' ''' I I " " I " '' I' " ‘ I m/z 71.00 81.31% Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51010: Hexacosane 57

5000 85 37.00 37.20 3740 m/z 85.05 60.61% 295 366 "r T I'''' I''' ‘ I ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #44318: Docosane 57 <■', t". I'f

85 37,00 37.20 37.40 37.60 5000 "m/z 43.05 56.41%

nfe-> JJjXiXx 266 p”’ ’' I 310 I'''' I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 ^bundance #49558: Heptadecane, 9-octyl- 57 37.00 37.20 37.40 37.60 "mTz 41705 36.98% Saw 85

Il I ”3 141 169 239 310 352 I'"' I" "V"' I'"' I I'''' I' ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 37.00 37.20 37.40 37.60

23320.D NP091101.M Mon Oct 15 09:54:10 2001 Page 18

NYC-WTC_000088231

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NYC-WTC_000088231Source: NYC Law Department, mirrored locally

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