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GC/MS analysis results for sample AD23320, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23320 conducted on October 15, 2001.

NYC-WTC_000088207–000088236

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088232
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT1201\23320.D Vial: 13 Acq On : 12 Oct 2001 1:51 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 19 Dotriacontane Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 38.36 0.79 ug/1 75298 Perylene-dl2 37.22 Hit# of 5 Tentative ID MW MolForm CAS# Qual .

1 Dotriacontane 451 C32H66 000544-85-4 91, 2 Tetratriacontane 479 C34H70 014167-59-0 91 3 Hexatriacontane 507 C36H74 000630-06-8 91 4 Pentatriacontane 493 C35H72 000630-07-9 91 Abundance Scan 3630 (38.361 min): 23320.D (-) "m/z SYTOO 100.00% 5(7

85 5000

38.00 38.20 38.40 38.60

s m/ z 71.10 82.46% ■nfe-> 50 100 150 200 250 300 350 400 450 500 Abundance #74491: Dotriacontane 57

5000 85 38.00 38.20 38.40 38.60 “mTz 43.05 68.19% 196 281 ^7 tVz-> 50 100 150 200 250 300 350 400 450 500 <\bundance #58265: Tetratriacontane 57

38.00 38.20 38.40 38.60 5000 85 m/z 85.05 52.45%

311 367 410 ■nfe-> 50 100 150 200 250 300 350 400 450 500 Abundance #59136: Hexatriacontane 7 38.00 38.20 38.40 38.60 “m/z 55700 23.12%

5000- 85

.. IJ .L f 7. I.. .... I.... I. A Tl/Z-> 50 100 150 200 250 300 350 400 450 500 38.00 38.20 38.40 38.60

23320.D NP091101.M Mon Oct 15 09:54:12 2001 Page 19

NYC-WTC_000088232

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NYC-WTC_000088232Source: NYC Law Department, mirrored locally

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