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GC/MS analysis results for sample AD23320, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23320 conducted on October 15, 2001.

NYC-WTC_000088207–000088236

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088233
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT1201\23320.D Vial: 13 Acq On : 12 Oct 2001 1:51 pm Operator: 2 09 GTkLOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 20 Dotriacontane Concentration Rank 15 R.T. EstConc Area Relative to ISTD R.T. 39.61 0.72 ug/1 68757 Perylene-dl2 37.22 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Dotriacontane 451 C32H66 000544-85-4 9L 2 Pentatriacontane 493 C35H72 000630-07-9 91 3 Triacontane 422 C30H62 000638-68-6 90 4 Heneicosane, 11-(1-ethylpropyl) -____ 366 C26H54 055282-11-6 90 Abundance c7 Scan 3766 (39,610 min); 23320,D {-) 7n7z 56795 100.00%

85 5000

■n/z-> JL 50 100 150 200 250 281

300 350 400 450 39,20 39,40 39,60 39,80 40,00 ■m/z 71.00 74740% Abundance #74491: Dotriacontane 57

5000 85 39,20 39,40 39,60 39,80 40,00 m/z 43705 68777% J ■196....... 281.............. ■n/z-> 50 100 150 200 250 300 350 400 450 Abundance #58743: Pentatriacontane 57

39,20 39,40 39,60 39,80 40,00 5000 85 ■m/z 85705 50.68%

J ll^ 1]'',]^,,141 169, 197,^5.................................................... Ti/z-> 50 100 150 200 250 300 350 400 450 Abundance #55461: Triacontane 4)3 39,20 39,40 39.60 39.80 40,00 m/z 69.05 24.66% 71

99 ‘ Il I ,7 ..... ..... .... , Tl/z-> 50 100 150 200 250 300 350 400 450 39,20 39,40 39,60 39,80 40,00

23320.D NP091101.M Mon Oct 15 09:54:14 2001 Page 20

NYC-WTC_000088233

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NYC-WTC_000088233Source: NYC Law Department, mirrored locally

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