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GC/MS analysis results for sample AD23271, Oct 15 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23271 conducted on October 15, 2001.

NYC-WTC_000088372–000088401

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088394
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23271.D Vial: 19 Acq On : 12 Oct 2001 7:43 pm Operator; 209 GTkLOS Sample ; gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DAT7kBASE\NBS75K.L ********************************************************************* Peak Number 16 Hexatriacontane Concentration Rank 7

R.T. EstConc Area Relative to ISTD R.T. 35.50 5.24 ug/1 479543 Perylene-dl2 37.23 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 94 2 Heneicosane 296 C21H44 000629-94-7 91 3 Tetratetracontane 619 C44H90 007098-22-8 91 4 Heptadecane, 9-octyl- 352 C25H52 007225-64-1 9L Abundance Scan 3318 (35.499 min); 23271 .D (-) m/z 57.00 100.00% 57

5000 85

35.20 35,40 35.60 35.80 ,, , 211239267295, ,,,,,, , , . , , , , , , , , , . ... . , m/z 71.10 71.04% ■n/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #74636: Hexatriacontane 57

5000- 85 _____________________ 35.20 35.40 35.60 35.80 m/z 43.05 63.16% , I . ■ . . ....... . I..... ........ . , ........I , A Ti/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #42201: Heneicosane 57

85 T-Ft

m/z A 35.20 35.40 35.60 35.80 85.05 49.66% 5000

■n/z-> Abundance 50 iw 100 150 ............. 268296 200 250 300 350 400 #61068: Tetratetracontane 450 500 550 600

7 35.20 35.40 35.60 35.80 m/z 55.00 23.99% 5000 85

69.197225 379407 590618 Tlfe-> 50 100 150 200 250 300 350 400 450 500 550 600 35.20 35;40 Ss'sO Ss'sO

23271.D NP091101.M Mon Oct 15 09:38:12 2001 Page 16

NYC-WTC_000088394

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NYC-WTC_000088394Source: NYC Law Department, mirrored locally

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