GC/MS analysis results for sample AD23271, Oct 15 2001

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Library Search Compound Report ■Data File : C:\HPCHEM\1\DATA\OCT1261\23271.D Vial: 19 Acq On : 12 Oct 2001 7:43 pm Operator: 209 GTkLOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15. Hexatriacontane Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 34.61 5.32 ug/1 577853 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Hexatriacontane 507 C36H74 000630-06-8 94 2 Octadecane 254 C18H38 000593-45-3 91 3 Heneicosane 296 C21H44 000629-94-7 9T 4 Pentacosane 352 C25H52 000629-99-2 91 Abundance Scan 3221 (34.609 min); 23271 .D (-) m/z 57700 100.00% 57

5000 85

4- I ' ' ' ' I ■p“ 34.20 34.40 34.60 34.80 35.00 169 197 225 267 295 380 “mTz 71.00 72.01% ' I" > • I" " I" " I" " r "' I' ’" I" " I" " I" " r "' I" ’' I" Ti/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #74636: Hexatriacontane 5(7

5000 85 34S 34^2376O 5S^^ m/z43.05 64.13%

Tite-> 40 60 MX 141 169 197 ‘' i'''' I'''' I'''' I' I" ' ‘ I'''' I'''' I'''' I " '' I'''' r ''' I'"' I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #71561: Octadecane 57

34.20 34.40 34.60 34.80 35.00 85 5000 “m/z 85.05 48.97%

224 2^ I" " I I j JT. I I . I I 111 iTr| I'''' I ‘' I'''' I nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #42201: Heneicosane I tC-i r-| . I . 71 , . , , I . I I I I i 1 57 34.20 34.40 34.60 34.80 35.00 "mTz 55.00 23.04% 85 5000

113 .XI

■n/z-> JU4 268 296 I'''' I'' " I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 I'''' I " '' I T T 34.20 34.40 34.60 34.80 35.00

23271.D NP091101.M Mon Oct 15 09:38:10 2001 Page 15

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