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GC/MS analysis results for sample AD23271, Oct 15 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23271 conducted on October 15, 2001.

NYC-WTC_000088372–000088401

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088392
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23271.D Vial: 19 Acq On : 12 Oct 2001 7:43 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 Hexatriacontane Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 33.69 6.98 ug/1 758030 Chrysene-dl2 33.12 Hit# Of 5 Tentative ID MW MolForm CAS# Qual (iJHexatriacontane 507 C36H74 000630-06-8 94 2 Octadecane 254 C18H38 000593-45-3 91 3 Heneicosane 296 C21H44 000629-94-7 91 4 Eicosane, 7-hexyl-___________________ 366 C26H54 055333-99-8 91 Abundance Scan 3121 (33.691 min): 23271. D (-) m/T 57.00 100.00% 5|7 ft 5000 85

4 Ji n/z-> Abundance XUh 40 60 I/r J 151 . 169 .197 225 253 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 #74636: Hexatriacontane 281 323 I'''' I'''' I 366 33.40 33.60 33.80 34.00 m/z 71.00 77761%

57

5000 85 ' T I . I I r |- 33.40 33.60 33.80 34.00 m/z43.05 65.63%

n/2-> Abundance 40 60 uu I.P _ 141 169 197 rTVTpVrTfTTTrp-rTTpTTTTTTTTYrrrrprrTTpTTTT^ 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 #71561; Octadecane 57 ,... ............ 33.40 33.60 33.80 34.00 85 in/z 85.05 49.49%

' ‘ 1'' '' I' ''' I' ‘ ‘ ‘ I'''' I''' ' I ‘' I'''' I'''' I'''' I'''' I' ‘' I'' '' I'''' I'''' I'''' I'' n/z-> Abundance 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 57 #42201: Heneicosane L "'"M 33.40 33.60 33.80 34.00 m/z 41705 24770% 85 553

■nfe-> T-q-TT ..1 I 113 izi i'''' I'''' I'''' I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 268 296 I'''' I''' 11' I'''' I'' ‘' I A 33.40 33.60 33.80 34.00

23271.D NP091101.M Mon Oct 15 09:38:07 2001 Page 14

NYC-WTC_000088392

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NYC-WTC_000088392Source: NYC Law Department, mirrored locally

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