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GC/MS analysis results for sample AD23318, Oct 15 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23318 conducted on October 15, 2001.

NYC-WTC_000088402–000088428

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088420
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23318.D Vial: 20 Acq On : 12 Oct 2001 8:42 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Hexatriacontane Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 33.69 4.55 ug/1 481337 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 94 2 Tetratetracontane 619 C44H90 007098-22-8 9h 3 Heneicosane 296 C21H44 000629-94-7 91 4 Heptadecane 240 C17H36 000629-78-7 91 Abundance Scan 3121 (33.689 min): 23318.D (-) m/z 57.00 100.00% 5/

5000 85 V I 1 j rr? f’’,169197225253281309 : 33.40 33.60 33.80 34.00 366 m/z 71.05 72.79% ' I '" ' ' 1 ’ ' ' ' I '' ' ' I ■ ’'' I ' ' ' ' I ' ' ' ' I n^-> 50 100 150 200 250 300 350 400 450 500 550 600 <\bundance #74636: Hexatriacontane 57

5000 85 JV, 33.40 33.60 33.80 34.00 m/z43.05 64.35% ........................... TiZz-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #61068: Tetratetracontane 57

33.40 33.60 33.80 34.00 5000 m/z 85705 49.10% 85

I fP,^f\169l97225 379407 590618 I IV ' '' I 11 ''i (' ' ‘‘ I ' ' ' ' I ' ' ‘ ‘ i ' ' ' ' I ' ' ' ' I ‘ ' I ' ' ' ' I ' ' ' ' I ' ' m/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #42201: Heneicosane V' ' T c7 33.40 33.60 33.80 34.00 m/z 41705 23.75% 85 5000

■n/z~> 50 100 150 200 250 300 350 400 450 500 550 600 33.40 33.60 33.80 34.00

23318.D NP091101.M Mon Oct 15 09:46:05 2001 Page 12

NYC-WTC_000088420

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NYC-WTC_000088420Source: NYC Law Department, mirrored locally

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