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GC/MS analysis results for sample AD23318, Oct 15 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23318 conducted on October 15, 2001.

NYC-WTC_000088402–000088428

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088421
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23318.D Vial: 20 Acq On : 12 Oct 2001 8:42 pm Operator: 209 ‘GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ************************************************************************** Peak Number 13 Hexatriacontane Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 34.61 3.47 ug/1 367563 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual.

1 Hexatriacontane 507 C36H74 000630-06-8 9^ 2 Heneicosane 296 C21H44 000629-94-7 91 3 Tetracosane 338 C24H50 000646-31-1 91 4 Pentacosane ____________________ 352 C25H52 000629-99-2 9T Abundance Scan 3221 (34.607 min): 23318.D (-) m/z 57.00 100.00% 5f7 71 43 85 5000-

I 99 I .'P, ,f) , I'k, ,,,,,,, I,,,, I, 34.20 34.40 34.60 34.80 35.00 Wz 71.00 71742% Tl/z-> Abundance 40 60

43 57 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #74636: Hexatriacontane J 5000 71 85 .. / L.... 34.20 34.40 34.60 34.80 35.00 m/z43.05 64.22%

TiZ2-> J ' H T ?7141155169183197211_________________ ' 1 ” T-TT'YT-rrT-yT'rTTYTTTryTT^rTjTTTTp-rTTyrTT-ryTTTTprTTT^^ 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #42201: Heneicosane 57 71 85 34.20 34.40 34.60 34.80 35.00 5000 m/z 85.05 50.77% 99 J ^]®^fl41156 268 296 ■|««TIJ111«I.«»« I»I n 11»k I ‘1 ’ I ’ Ti/z-> Abundance 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #73543; Tetracosane /I ....... 43 57 34.20 34.40 34.60 34.80 35.00 71 ■m/z 5^700 23.52%

5000 85

99 l| ’’,1^127 155169183197 I ' ' 1 I' 294 338 I I I I < I I I « ( I I I I I I I IT I I I t I I <' I < 1' ’ ’' I ’ ‘I ’ Tl/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 34.20 34.40 34.60 34.80 35.00

23318.D NP091101.M Mon Oct 15 09:46:07 2001 Page 13

NYC-WTC_000088421

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NYC-WTC_000088421Source: NYC Law Department, mirrored locally

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