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GC/MS analysis results for sample AD23318, Oct 15 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23318 conducted on October 15, 2001.

NYC-WTC_000088402–000088428

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088422
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23318.D vial: 20 Acq On : 12 Oct 2001 8:42 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 Heneicosane Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 35.50 3.51 ug/1 304164 Perylene-dl2 37.22 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 91 2 Pentacosane 352 C25H52 000629-99-2 91 3 Nonacosane 408 C29H60 000630-03-5 91 4 Heneicosane, 11-(1-ethylpropyl)- 366 C26H54 055282-11-6 91 4bundance Scan 3318 (35.498 min): 23318.D (-) m/z SYTOO 107700% 57

5000 85

35.20 35.40 35.60 35.80 " I" " I" ’' I m7z 71.00 72768% Tife-> Abundance 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 #42201: Heneicosane J 57

85 5000 35.20 35.40 35.60 35.80 m/z 41705 67766% 1113

Ti/z-> JjjLXaXh I , i‘l. I Ti I ."| I. T. I .f 11, J I''" I"'' I “ " I"'' r " ‘ I'" 11"'' I" " I" “ i'"' I"' ‘ I''" I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 Abundance #73718; Pentacosane 43

71 35.20 35.40 35.60 35.80 5000 m/z 85.05 49.12%

, 99

■n/z-> XU I 127 155 183 211 40 60 80 100 120140 160 180 200 220 240 260 280 300 320 340 360 380 400 I " '' I " " I "'' I

Abundance #54526: Nonacosane ................. 43 35.20 35.40 35.60 35.80 m/z 54.95 23.73% 71 A 5000

■n/z-> I'' " I' " ' I " " I' “ ‘ I 211 239 p ''' 1" " p ' 40 60 80 100 120 140 160180 200 220 240 260 280 300 320 340 360 380 400 379 408 pTTTp-TTTpTTTJ JV 35.20 35.40 35.60 35.80

23318.D NP091101.M Mon Oct 15 09:46:10 2001 Page 14

NYC-WTC_000088422

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NYC-WTC_000088422Source: NYC Law Department, mirrored locally

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