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GC/MS analysis report for sample AD22546, September 2001

Machine-extracted title · confidence 95%

Laboratory results for sample AD22546 indicating other unknown compounds detected via GC/MS on September 27, 2001.

NYC-WTC_000086949–000086971

Folder label: “508 Scan 9/17/01 9/26/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2501\22546.D Vial: 12 Acq On : 26 Sep 2001 1:14 am Operator: 209 GALOS Sample : GC/MS unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Heneicosane Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 35.53 1.06 ug/1 145989 PerYlene-dl2 37.27 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 91 " 2 Octadecane 254 C18H38 000593-45-3 91 3 Pentacosane 352 C25H52 000629-99-2 91 . 4 Nonacosane 408 C29H60 000630-03-5 91 Abundance Scan 3321 (35.528 min): 22546.D (-) m/z SYTOO 100.00% 71 43 85 5000

99 ■n" 35,20 3540 35J0 35J0 141 155169183 207 239 253 283 I ' '' ' ' I ' ' ' ' i ' ' ' ' I ' ' ' ' I ' ' ' ' I ' m/z 71.00 71.77% n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #42201: Heneicosane 57 71 85 5000 35.20 35.40 35.60 35.80 99 m/z 43.05 63.70% 127 141 155 ', I 1 268 296 I ' ' ' ' I ' '' I I nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #71561: Octadecane 57 43 71 35.20 35,40 35,60 35.80 85 c 553 mTz 85.00 50.03%

224254 Tife-> 40 -JU 60 J- 'I ' ' ' ‘ I • ' I I I • ' • • I 80 100 120 140 160 180 200 220 240 260 280 300 I ''' ' I ' ' ' ' I

^bundance #73718: Pentacosane ' I' ' ' ' I ' ' ' ' I 4t3 5|7 35.20 35.40 35.60 35.80 m/z 55.00 24.37% 71 5000 85

n/z-> J7"^ 40 60 141 155 169 183 197 211 225 ¥YrT-tnq-r-‘rT*r-]H-r-rrj-T-rn-T-yv-r-rT-y^ ■p I 1 I 80 100 120 140 160 180 200 220 240 260 280 300 35.20 35.40 35.60 35.80

22546.D NP091101.M Wed Oct 03 14:44:48 2001 Page 12

NYC-WTC_000086968

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NYC-WTC_000086968Source: NYC Law Department, mirrored locally

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