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GC/MS analysis report for sample AD22546, September 2001

Machine-extracted title · confidence 95%

Laboratory results for sample AD22546 indicating other unknown compounds detected via GC/MS on September 27, 2001.

NYC-WTC_000086949–000086971

Folder label: “508 Scan 9/17/01 9/26/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2501\22546.D Vial: 12 Acq On : 26 Sep 2001 1:14 am Operator: 209 GALOS Sample : GC/MS unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L *********************************************************************** Peak Number 13 Eicosane Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 36.39 0.73 ug/1 100528 Perylene-dl2 37.27 Hit# of 5 Tentative ID MW MolForm CAS# Qual fyEicosane 282 C20H42 000112-95-8 94 ^2 Octadecane 254 C18H38 000593-45-3 90 3 Pentacosane 352 C25H52 000629-99-2 90 4 Heptadecane _____________________240 C17H36 000629-78-7 87 Abundance Scan 3415 (36.391 min): 22546.D (-) Wz 56795 100.00% 5(7

43 71 5000 85 7 99 "n" 36.00 36.20 36.40 36.60 36.80 .Il ,ll, .III I I I I'l I ^56 169 I , I ,■ i' I . I . I I . ."I I I 197209 253 281 m/z 71.00 63.20% Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 <\bundance #72326: Eicosane 57 43 71 5000 I 85 3ap0_3a20_ja40_3a60_36^ Wz 43.00 61.48% 99

Ti/z-> Uuu 40 60 I , , I', , ,'l, , 80 100 120 140 160 ..................................................... 282, 180 200 220 240 260 280 Abundance #71561: Octadecane 57 43 71 T 36.00 36.20 36.40 36.60 36.80 85 5000 m/z85.00 47.56%

I J 7TT711S5 224 254 Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 ^bundance #73718: Pentacosane 43 57 36.00 36.20 36.40 36.60 36.80 m/z 41705 22.01% 71 5000 85

I ■p I 12^41 155 169 183 197 211 225 m/z-> . 40 60 80 100 120 140 160 180 200 220 240 260 280 36.00 36.20 36.40 36.60 36.80

22546.D NP091101.M Wed Oct 03 14:44:50 2001 Page 13

NYC-WTC_000086969

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NYC-WTC_000086969Source: NYC Law Department, mirrored locally

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