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GC/MS analysis results for sample AD22779, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22779 conducted on October 5, 2001, identifying unknown compounds.

NYC-WTC_000087694–000087716

Folder label: “GC/MS Scan 9/20/01

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Scanned page image, NYC-WTC_000087712
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCTO 2O1\22779.D Vial; 16 Acq On 3 Oct 2001 4:48 am Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Eicosane Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 35.52 0.79 ug/1 102099 Perylene-dl2 37.28 Hit# Of 5 Tentative ID MW MolForm CAS# Qual Eicosane 282 C20H42 000112-95-8 93 Heptadecane 240 C17H36 000629-78-7 91 3 Heneicosane, 11-(1-ethylpropyl)- 366 C26H54 055282-11-6 91 4 Nonadecane 268 C19H40 000629-92-5 91 ^Kbundance Scan 3320 (35.522 min): 22779.D (-) Wz 57700 100.00% 57 71 43 5000 85

99 n ' ' ' I ' ' ' ■ I ' ' ' ' I 35.20 35.40 35.60 35.80 TT^M^Yrr+TyT^-TT-f-rT-i-ryTTVrp-r'rT'yTVrrpTT-rp-rT'TjVTT-TpT-rTyTTTTpT-TT^^ m/z 71.10 74.64% nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #72324: Eicosane 43 5(7

71 I I-PI I I /1 r-pfrpfv I 5000 85 35.20 35.40 35.60 35.80 m/z 43.05 61.37% Q9 J 113 141155169183197 254 282 ' I'''' I'''' r ''' I'''' I'''' I'''' I'''' I'''' I'''' I'''' I'''' I ‘' i'' Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #32063: Heptadecane 57

71 ' ' ' I ' ’ 85 35.20 35.40 35.60 35.80 5000 m/z 85.05 49744%

99

-TT-p-r nfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ^bundance #51002: Heneicosane, ll-(l-ethylpropyl)- 43 57 35.20 35.40 35.60 35.80 m7z 55.00 28.48% 71 5000 85

183197211225 295 338 1T I . I I ■ V ■ I . ’i ■ I I I I I' I”' Tl/Z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 35.20 35.40 35.60 35.80

22779.D NP091101.M Thu Oct 04 14:21:33 2001 Page 12 NYC-WTC_000087712

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NYC-WTC_000087712Source: NYC Law Department, mirrored locally

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