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GC/MS analysis results for sample AD23799, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23799 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089311–000089332

Folder label: “GC/MS Scan 10/1/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3001\23799.D Vial: 10 Acq On : 30 Oct 2001 11:19 pm Operator; 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title ; 209 625/TCLP calibration table Library : C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Eicosane Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 36.31 0.60 ug/1 140505 Perylene-dl2 37.16 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Eicosane 282 C20H42 000112-95-8Y9^ 2 Heneicosane 296 C21H44 000629-94-7 91 3 Hexatriacontane 507 C36H74 000630-06-8 91 - 4 Octadecane ____________________ 254 C18H38 000593-45-3 91 Abundance. Scan 3406 (36.309 min): 23799.D (-) m/z 57.00 100.00% 57 71 43 85

u 5000

' ' I ' ' ' ' I 1 J Ju J « I j I I I I I • 11 ' I I I I I I T I *1 I I I I I I I IT I I I I >' I I III j I r I I j I I I I I I 11" T I I *i I I j ‘ I "m “I I I m/z 36.00 36,20 36,40 36.60 71.10 78.85%

JL^ Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #72326: Eicosane 57 43 71 5000 85 36.00 36.20 36.40 36.60 m/z 43.05 64.74% 99

Tife-> ' ' I ' 40 J 60 80 ,1 141 155169 100 120 140 160 180 200 220 240 260 280 300' 282

Abundance___.. -----------------#42201 :.Heneicosane-------------------------- —---- --------- 57 71 85 36.00 36.20 36.40 36.60 5000 m/z 85.05 57.07% 99 268 296 I ' ' ' H ' ' ' ' I TiZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #74636: Hexatriacontane. , ._43-.5|7- -1.36.00 - 36.20-36.40 - 36.60 Wz 55710 307700% 71 5000 85.

., Ji. ....... '.... ......... ' Tlfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 36.00 36.20 36.40 36.60

23799.D NP103001.M Thu Nov 01 13:17:01 2001 . Page 13 ,

NYC-^CZ00M89330 ‘

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NYC-WTC_000089330Source: NYC Law Department, mirrored locally

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