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GC/MS analysis results for sample AD23799, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23799 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089311–000089332

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089329
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NYC 9/11 Public Portal Document

___ Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT3001\23799.D Vial: 10 Acq On : 30 Oct 2001 11:19 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L *******************★*****************************************'*'******* Peak Number 12 Hexatriacontane Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T. 35.45 0.98 ug/1 229536 Perylene-dl2 37.16 Hit# of 5 Tentative ID MW MolForm CAS#

1 Hexatriacontane 507 C36H74 000630-06-8(9^ 2 Pentatriacontane 493 C35H72 000630-07-9 9L 3 Tetratetracontane 619 C44H90 007098-22-8 91 4 Heneicosane 296 C21H44 000629-94-7 91 Abundance Scan 3312 (35.446 min): 23799.D (-) m/z 57.00 100.00% 57

85 5000

-J ,' If j |\ I.,., I,,,.,..., I. I.,,. I;, , , I , 35.20 35.40 35.60 35.80

TlZz-> 50 100 150 200 2^ 300 5^ 600 m/z 71.00 73.55% ‘ Abundance #74636: Hexatriacontane 57

5000 85 T 35.20 35.40 35.60 35.80 m/z 43.05 63.64%

nZz-> " so" ' iro ' 150 200 ' ' 250 " 300 " 3^ " 400 " 450 " 500 " 550 ' ' 600 Abundance----------------------------------------- #58743:. Pentatriacontane-------------------------------------- 57

35.20 35.40 35.60 35.80 5000 85 m/z 85.05 51.39%

Tife-> 50I 100 150 200 250 300 3^ 500 550 600 Abundance .„ . #61068: Tetratetracontane 57 ^=^35.20- 35.40 - 35.60 - 35.80—. m/z 55.00 23 ;83% A 5000 85

, I* ....................... I .. I........................... '' I ' ■nZz-> 50 100 150 200 250 300 350 400 450 500 550 600 35.20 35.40 35.60 35.80

23799.D NP103001.M Thu Nov 01 13:16:59 2001 Page 12

NYC-WTC_000089329

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NYC-WTC_000089329Source: NYC Law Department, mirrored locally

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