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GC/MS analysis results for sample AD23500, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23500 conducted on October 19, 2001.

NYC-WTC_000088826–000088852

Folder label: “GC/MS Scan 9/27/01

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NYC 9/11 Public Portal Document

Library Search-Compound-Report Data File : C:\HPCHEM\1\DATA\OCT1601\23500.D Vial: 8 Acq On : 16 Oct 2001 9:05 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 15 Hexatriacontane Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 35.50 2.71 ug/1 225487 Perylene-dl2 37.23 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Heneicosane 296 C21H44 000629-94-7 91\ 3 Pentacosane 352 C25H52 000629-99-2 91/ 4 Heptadecane, 9-octyl- 352 C25H52 007225-64-1 93/ Abundance Scan 3318 (35.503 min): 23500. D (-) m/z 57.00 100.00% 7 71 43 5000 85

JJU 99 35.20 35.40 35.60 35.80 J|[ ,lj l-T-Y'4‘4nH*"prr^TyT**¥-rT-p-Tn-^q-T-T"TT-yVT-T-T-y-rTT-q-^^ m/z 71710 69.46% ' I ' ‘ ' I ' nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #74636: Hexatriacontane 43 5 7

71 5000 85 35.20 35.40 35.60 35.80 Wz 43705 62715% 97 l| , 155 169 183 197,211 ' ' I ' ' '' I ' ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance--------------- ---------------- -— — #42201: Heneicosane 57 71 WT-T

85 35.20 35.40 35.60 35.80 5000 m/z 85.05 49.04% 99

■nlz-> Abundance '' I' 40 UJJUte: 60 80 100 120 140 160 #73718: Pentacosane 180 200 220 240 260 280 300 268 296 I • I I • I ' • ■' 11 • I I I '

... _ 43-5,7 - 35.20 35:40 35.60 - 35.80 m/z 41.05 24.73% 71 5000 85

nZz-> ■'N' 40 u 60 Il I ' ' ' ' I 80 I, T 1?7141 155 169 183 197 211 225 ' ' I ' ' ' ' I ' ' ' ' f' ' ' I ' ' I ' ' ‘ ' I ' ' ' ' I ‘ ‘ 100 120 140 160 180 200 220 240 260 280 300 ' I ' ' ' ‘ I ' ' 35.20 35.40 35.60 35.80

23500.D NP091101.M Thu Oct 18 10:18:13 2001 Page 15

NYC-WTC_000088847

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NYC-WTC_000088847Source: NYC Law Department, mirrored locally

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