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GC/MS analysis results for sample AD22580, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22580 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087202–000087225

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087221
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2801\22580.D Vial: 8 Acq On : 28 Sep 2001 7:17 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 13 Hexatriacontane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 35.53 1.05 ug/1 172124 Perylene-dl2 37.29 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Pentacosane 352 C25H52 000629-99-2 90 3 Heneicosane 296 C21H44 000629-94-7 90 / 4 Octadecane ____________________ 254 C18H38 000593-45-3 90 / ^bundance Scan 3321 (35.531 min): 22580.D (-) m/z ^.00 100.00% 57 71 I 43 85 5000

99 I ‘ '

Ti/z-> JUUuL 40 60 80 ,|J

100 120 140 160 169183 197211

180 200 220 253

240 260 280 283

300 35,20 35.40 35.60 35.80 m/z71.00 69.34% Abundance #74636: Hexatriacontane 43 57

71 / 5000 85 T 35.20 35.40 35.60 35.80 m/z 43.05 60.72% 97 , ,H, 1??,^'*.'*, ■nfe-> 40 60 80 100, 120 140 160 180 2(ro ao ' 2^ 280 300 Sundance #73718: Pentacosane 43 5,7

71 35.20 35.40 35.60 35.80 5000 m/z 85.05 50.57% 85 ft

JU 1^169 183197 211 225 Ti/z-> Abundance 40 60

57 80 100 120 140 160 180 200 #42201: Heneicosane 220 240 2fi0 9Rn 300 R ;^.2O 35.40 35.60 35.80 71 m/z 41.05 23741% A 85 5000

99 I 113 127141 155 ■Ur 268 296 . ................ . T ■n/z~> 40 60 80 100 120 140 160 180 200 2^ 240 260^^0 300 35.20 35.40 35.60 35.80

22580.D NP091101.M Wed Oct 03 11:38:03 2001 Page 13

NYC-WTC_000087221

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NYC-WTC_000087221Source: NYC Law Department, mirrored locally

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