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GC/MS analysis results for sample AD23843, Nov 2 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23843 conducted on November 2, 2001, identifying unknown compounds.

NYC-WTC_000089397–000089417

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089417
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT3001\23843.D Vial: 15 Acq On : 31 Oct 2001 4:11 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L *********************************** ******************** 4: ***** it ****** * Peak Number 13 Hexatriacontane Concentration Rank 8 R.T. EstConc Area Relative to ISTD R.T. 36.31 0.86 ug/1 176313 Perylene-dl2 37.17 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Heptadecane 240 C17H36 000629-78-7 91 3 Pentacosane 352 C25H52 000629-99-2. 91 4 Octadecane _______ 254 C18H38 000593-45-3 90 Abundance Scan 3406 (36.311 min): 23843.D (-) m/z SYTOO 100.00% 57

43 71 85 5000

nZz-> Abundance uu 40

43 57 60 ..,.lll, .I,l ¥YT'TTTyrT*TT-YT‘VTn-fTnrrir7Tr+TT^YVTT‘xjT-rTxyTTTT^^ 80 1. 113 100 120 140 160 #74636: Hexatriacontane 180 .__________ 253 200 220 240 260 281 280 36.00 36.20 36.40 36.60 ra/z71.10 70.12%

71 5000 85 I i|WT I I r I I I I I I

36.00 36.20 36.40 36.60 m/z 43705 66728% 97

TiZz-> 40 J60 I 80II 100 jl IP 197 211 I ' ' ' ' I I ' ' ' I ' ' I . I I . . . i'. . . I I . . . . I , , , . I . . . , I , , ' ' I ' ' ’ ' I ' ' ' ' I ' ' 120 140 160 180 - 200 220 240 260 280 Abundance #71193: Heptadecane 57- T ik: T -r-r-r-p-r T 36.00 36.20 36.40 36.60 "n 71 253 m/z 85.05 51.62% 85

99 ..o -i^Lt?Ll41..1^.169; ,210— 240__ 'I''''I''''I' Ti/z-> 40 60 80 100 120 140 160. 180 200 220 240 260 280 Abundance #73718: Pentacosane ' ' I ‘ " I ^36.00-' 36;20 36.40 - 36.60 -m/z—55-700-- 26-0'4% 71 5000 85 —

■n&-> 40 □ 60 Il__ ip 127 141 155 169 183 197 211 225 I ' ' ' ' I ' ' ' ' I ' ' ' ' i'' ' ' '■ I ‘ 80 100 120 140 160 180 200 220 240 260 280 ' I ' ' ' ' I ' ' ' ' I ' ' 36.00 36.20 36 40 36 60

23843.D NP103001.M Thu Nov 01 14:45:46 2001 Page 13

NYC-WTC_000089417

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NYC-WTC_000089417Source: NYC Law Department, mirrored locally

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