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GC/MS analysis results for sample AD23125, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23125 conducted on October 12, 2001.

NYC-WTC_000088023–000088043

Folder label: “GC/MS Scan 9/24/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\OCT0401\23125 .D Vial: 13 Acq On 5 Oct 2001 3:16 am Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Hexatriacontane Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

36.39 0.71 ug/1 128143 Perylene-dl2 37.27

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Hexatriacontane 507 C36H74 000630-06-8 91 2 Heptadecane 240 C17H36 000629-78-7 91\ 3 Triacontane 422 C30H62 000638-68-6 91 \ 4 Pentacosane 352 C25H52 000629-99-2 91/ Abundance Scan 3415 (36.391 min): 23125.D (-) m/z 57.0^B 100.00% 5#

5000 85

M i '■' ' IT"'

bjUXu I Xil 3?^......... I,, hi/z->_____ 40 60 80 100 120140160 180 200 220 240 260 280 300 320 340 360 380 400 420 ....... 36.00 36.20 36.40 36.60 36.80 m/z 71.0,0 73.49% Abundance #74636: Hexafriacontane 57 "i'er'.'C'i n , , i^Y^Tpi-rt , I*,*,

5000 85 36.00 36.20 36.40 36.60 36.80 m/z 43.00 65.45% 1 11 , 141 169 197 I » I I 1 I T « I I I I I T I I I I « I p f I I I I , I » I I iTTp

m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance 57 #71193: Heptadecane

36.00 k' I ' ' 36.20 36.40 36.60 36.80 5000 i 85 m/z 85.0.5 46.94%

..j I 1 . . .......... ...... m/z-> 40 60 80 100 120140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 iAbundance #55461: Triacontane 4|3 36.00 36.20 36.40 36.60 36.80 m/z 41.05 22.05% 71 5000

i,................. T 239 267 I' ’ ‘' I" ’' I I" " I'"' I 379 422 ” r ''' I " " I' n m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 . 36.00 36.20 36.40 36.60 36.80

23125.D NP091101.M Tue Oct 09 12:44:41 2001 Page 12

NYC-WTC_000088041

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NYC-WTC_000088041Source: NYC Law Department, mirrored locally

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