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GC/MS analysis results for sample AD23500, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23500 conducted on October 19, 2001.

NYC-WTC_000088826–000088852

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088846
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23500.D Vial: 8 Acq On : 16 Oct 2001 9:05 pm Operator: 209 GALOS Sample : gc/ms unknoivn Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 Heneicosane Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 34.61 2.60 ug/1 262415 Chrysene-dl2 33.12 . Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 91 2 Eicosane, 7-hexyl- 366 C26H54 055333-99-8 91' 3 Heneicosane, 11-(1-ethylpropyl)- 366 C26H54 055282-11-6 91 4 Heptadecane, 9-octyl- 352 C25H52 007225-64-1 91 Abundance Scan 3221 (34.612 min); 23500.D (-) m/z 57700 100.00% 57 71 43 85 5000

T I I , ,1,, i .... ■m/z 34.20 34.40 34.60 34.80 35.00 71.00 72781% mfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #42201; Heneicosane 57

5000 71 85 I I 34.20 34.40 34,60 34.80 35.00 99 m/z43.05 66.77% 1.1, j I, n . IT111 j 11T11.. 1. 11.111 268 p-TTT-prrrtp 296

a I ' ' ' ' I '' '' I ' ' ' ' I mfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance _ #50999; Eicosane, _7-hexyl- _ _______________ 43 5)7

71 34.y 34.40 34.60 34.80 35.00 - 5000 85 ■m/z 85.05 50774% (1 281 310 ' IT■ 1 1 I I I I I I I ■ ■ ■ I ■ I ' r'''' I " " I ' I'' ' 'I ‘ I ' ’ ' ' I ' ' ' ' I TiZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #51002; Heneicosane, 1H 1_-^hylpropyl)-______ I 413 57' .34:20 34.40 34.60 34.80 35.00 “m/z 55700 23.90% 71 A 5000 , _85_ .

183197211225 338 r TT-p-r I ' ‘ ' ' I • ' ' I I I I I I j I i ' I ' ' ' ' I ' • ' r| i 1 ■nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 34.20 .34.40 34.60 34.80 35.00

23500.D NP091101.M Thu Oct 18 10:18:10 2001 Page 14

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NYC-WTC_000088846Source: NYC Law Department, mirrored locally

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