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GC/MS analysis results for sample AD23258, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23258 conducted on October 12, 2001.

NYC-WTC_000088048–000088068

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088061
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\OCT0901\23258.D Vial: 4 Acq On 9 Oct 2001 4:17 pm Operator: 209 GALOS Sample g c/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 7 Heneicosane Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 31.74 1.21 ug/1 223828 Chrysene-dl2 33.13 Hit# of 5 Tentative ID MW MolForm CAS# Qnal 1 Heneicosane 296 C21H44 000629-94-7 93, 2 Eicosane 282 C20H42 000112-95-8 91 3 Heptadecane, 9-hexyl- 324 C23H48 055124-79-3 91 4 Pentacosane 352 C25H52 000629-99-2 91 <\bundance Scan 2908 (31.741 min): 23258.D (-) m/z 57.00 100.00%

43 7 71 I 5000 85

T .1 1 ..i, .1 T 5^ ^^5169183197211225 31.40 31.60 31.80 32.00 281 m/z 71.00 66.00% I I 'p I n I I n I I ” I I r j I I T I I 'll I I p I II I ( r I I I ‘i I I r" J I I I I I I I I I I I I I p-n-rp- 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #42201: Heneicosane 5)7 71

r' H, a I 85 5000 ' I 31,40 31,60 31,80 32.00 99 m/z 43.05 65.96% 268 296 I ' ' ' ' p ' ' 'I I I T I p ' ' I I I ' I I I I I ' • • p • • • p ' ' ‘ I I ‘‘ I' '' 11 7i/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #72323: Eicosane 43 7

31.40 31.60 31.80 32.00 71 5000 m/z 85.00 47.13% 85

282 I''' • I' < ‘' p • ’' p''' I

A ' ! ' ' I ' 1 * ' ' ' I ' ■n^-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 Abundance #46162: Heptadecane, 9-hexyl- 413 57 31.40 31.60 31.80 32.00 m/z 41.05 24.46% 71 A 5000 85

239 296 324 ... T^pT-VT-q-rVrT-jH- p '' ' p ' ‘' I''' • p ''' p I'' r*'' * I ‘‘' I''' T ■n/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 31.40 31.60 31.80 32.00

23258.D NP091101.M Thu Oct 11 10:41:11 2001 Page 7

NYC-WTC_000088061

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NYC-WTC_000088061Source: NYC Law Department, mirrored locally

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