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GC/MS analysis results for sample AD23473, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23473 conducted on October 19, 2001.

NYC-WTC_000088725–000088752

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000088745
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C;\HPCHEM\1\DATA\OCT1601\23473.D Vial: 4 Acq On ; 16 Oct 2001 5:10 pm Operator: 209 GALOS Sample ; gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 14 Heneicosane Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 34.61 4.41 ug/1 511830 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Heneicosane 296 C21H44 000629-94-7 91 2 Octadecane 254 C18H38 000593-45-3 91\ 3 Tetracosane 338 C24H50 000646-31-1 90p 4 Eicosane 282 C20H42 000112-95-8 9(Z Abundance Scan 3221 (34.608 min): 23473.D (-) m/z 57700 100.00% 57

43 71 85 5000

99 R 34.20 34.40 34.60 34.80 35.00 I i, iJ \r''r^^\''.?^1?9.^83197211225239253267281 ' I " '' I'' ■m/z 71.00 69.68% n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #42201: Heneicosane 57 71 85 5000 34.20 34.40 34.60 34.80 35.00 99 "mTz 43700 64784% I ■ n . I r... I..T, 111.. I., I,I 268 296 I " " I ' " ' I' mfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71561: Octadecane 5t7' . ...... ;.... ..... . 43 71 34.20 34.40 34'50 34'.80 35W 85 5000 m/z 85.05 50.42%

m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 7'43 57 - 34.20 ~34.40 34.60 34.80 35.00 71 "m/z 55.00 23.92%

5000 85

99 .., IT11,111.. 111.. I,, .■‘i I. r 1.111 294 338 I'''' I'''' r ''' I'''' I'''' I'''' I' J TlZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 34.20 34.40 34.60 34.80 35.00

23473.D NP091101.M Wed Oct 17 13:17:51 2001 Page 14

NYC-WTC_000088745

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NYC-WTC_000088745Source: NYC Law Department, mirrored locally

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